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Call for Papers - JMR Focus Issue
Indentation Methods in Advanced Materials Research


Enormous progress in the field has been achieved in the last decade, made possible both by advances in instrumentation as well as improved modeling capabilities. The purpose of this special focus issue of Journal of Materials Research is to present recent state of the art developments. To be considered for the issue, manuscripts must be submitted by July 31. Find out more...
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In-situ TEM Study of Bismuth Nanostructures
Xiaoting Jia, Vincent Berube, Shuo Chen, Bed Poudel, Son Hyungbin, Jing Kong, Yang Shao-Horn, Ren Zhifeng, Gang Chen, Mildred S Dresselhaus
From MRS Proceedings Volume 1044

Abstract: Nanostructured thermoelectric materials have attracted lots of interest in recent years, due to their enhanced performance determined by their thermoelectric dimensionless figure of merit. However, because of equipment limitations, not much work has been done on combining simultaneous transport measurements and structural characterization on individual nanostructured thermoelectric materials. With an integrated TEM-STM system, we studied the structural behavior and electrical properties of bismuth (Bi) nanobelts and nanoparticles. Results showed that clean Bi nanostructures free of oxides can be produced by in-situ high temperature electro-migration and Joule annealing processes occurring within the electron microscope. Preliminary electrical measurements indicate a conductivity of two orders of magnitude lower for Bi nanoparticles than that for bulk Bi. Such in-situ studies are highly advantageous for studying the semimetal-semiconductor transition and how this transition could enhance thermoelectric properties.

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