Symposium TC02: In Situ Studies of Materials Transformations

2017-11-27   Show All Abstracts

Symposium Organizers

Yuzi Liu, Argonne National Laboratory
Daan Hein Alsem, Hummingbird Scientific, Inc
Yugang Sun, Temple University
Lin Wang, Center for High Pressure Science and Technology Advanced Research

Symposium Support

Direct Electron, LP
Gatan, Inc.
TC02.01: In Situ HR(S)TEM
Session Chairs
Matthew Kramer
Yuzi Liu
Monday AM, November 27, 2017
Hynes, Level 2, Room 200

8:00 AM - TC02:01.01
In Situ HRTEM Observation of hcp → Periodic Structures → fcc Phase Transformation of Ti Precipitates in Nb-Ti-Si Based Alloys

Xiao Ma 1 , Xiping Guo 1 , Maosen Fu 1
1 State Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi'an China

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8:15 AM - TC02:01.02
In Situ Transmission Electron Microscopy Observations of the fcc-hcp Phase Transformation in Co Nanowhiskers

Gunther Richter 1 , Wenting Huang 1
1 , Max Planck Institute Intelligent Systems, Stuttgart Germany

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8:30 AM - *TC02:01.03
TEM and X-Ray Nanoprobe Studies of Nanoscale Resistive-Switching Oxide Heterostructures

Amanda Petford-Long 1 2 , Daniel Hong 1 3 , Charudatta Phatak 1
1 , Argonne National Laboratory, Lemont, Illinois, United States, 2 Materials Science and Engineering, Northwestern University, Evanston, Illinois, United States, 3 Materials Science and Engineering, KAIST, Daejeon Korea (the Republic of)

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9:00 AM - TC02:01.04
Synthesis and In Situ Alloying of Bimetallic Nanorods

Jessi van der Hoeven 1 , Tiago da Silva 2 , Wiebke Albrecht 1 , Tiansong Deng 3 , Catherine Louis 2 , Alfons van Blaaderen 1 , Petra de Jongh 1
1 Debye Institute for Nanomaterial Science, Utrecht University, Utrecht Netherlands, 2 , Université Pierre et Marie Curie – UPMC, Paris France, 3 , The University of Chicago, Chicago, Illinois, United States

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9:15 AM - TC02:01.05
In Situ Observation of the Formation and Migration of Defects in MoSe2/Graphene van der Waals Heterostructures

Carlos Alvarez 1 , Pascal Pochet 1 , Minh Dau 1 , Alain Marty 1 , Celine Vergnaud 1 , Helene Le Poche 2 , M. Jamet 1 , Hanako Okuno 1
1 , Univ Grenoble Alpes, CEA, INAC, Grenoble France, 2 , Univ. Grenoble Alpes, CEA, LITEN, Grenoble, 38000, France

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9:30 AM - *TC02:01.06
Real-Time Atomic Scale Imaging of Amorphous-Crystalline and Crystalline-Crystalline Phase Transformations

Matthew Kramer 2 1 , Lin Zhou 2 , Fanqiang Meng 2 , Ryan Ott 2 , Ralph Napolitano 2 1
2 Division of Materials Science and Engineering, Ames Laboratory, Ames, Iowa, United States, 1 , Iowa State University, Ames, Iowa, United States

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10:00 AM -
BREAK

10:30 AM - *TC02:01.07
In Situ Observation of Shear-Driven Amorphization Process in Silicon Crystals

Scott Mao 1
1 Department of Mechanical Engineering and Materials Science, University of Pittsburgh, Pittsburgh, Pennsylvania, United States

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11:00 AM - TC02.01.08
Direct Observation of the Reaction Mechanism of Ni/6H-SiC and Behavior of Carbon at Low Temperature by In Situ Transmission Electron Microscopy

Yena Kwon 1 , Cheol-Woong Yang 1
1 , Sungkyunkwan University, Suwon Korea (the Republic of)

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11:15 AM - TC02:01.09
How a Cation Exchange at Solid State between Diverse Nanoparticles Populations Occurs—New Insights by In Situ HRTEM and STEM-EDS Imaging

Andrea Falqui 1 , Alberto Casu 1 , Davide Deiana 2 , Hongbo Li 3
1 , King Abdullah University of Science and Technology, Thuwal Saudi Arabia, 2 Centre Interdisciplinaire de Microscopie Electronique, Ecole Polytechnique Federale de Lausanne, Lausanne Switzerland, 3 Chemistry Department, Los Alamos National Laboratory, Los Alamos, New Mexico, United States

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11:30 AM - TC02:01.10
Direct Exchange of Re and Mo Atoms in Monolayer MoS2

Shize Yang 1 , Weiwei Sun 2 , Yu-Yang Zhang 2 , Yongji Gong 3 , Matthew Chisholm 1 , Sokrates Pantelides 2 , Wu Zhou 4
1 , Oak Ridge National Laboratory, Oak Ridge, Tennessee, United States, 2 , Vanderbilt University, Nashville, Tennessee, United States, 3 , Beihang University, Beijing China, 4 , University of Chinese Academy of Sciences, Beijing China

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11:45 AM - TC02:01.11
Dislocation Aided Particle Alignment Controls Coalescence During the Initial Stages of Crystal Growth

Amit Samanta 1 , Andrew Lange 1 , Tammy Olson 1 , Selim Elhadj 1
1 , Lawrence Livermore National Laboratory, Livermore, California, United States

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TC02.02: Liquid TEM
Session Chairs
Yugang Sun
Haimei Zheng
Monday PM, November 27, 2017
Hynes, Level 2, Room 200

1:30 PM - *TC02.02.01
Nanomaterials Transformations and Dynamic Phenomena at Solid-Liquid Interfaces

Haimei Zheng 1
1 , Lawrence Berkeley National Laboratory, Berkeley, California, United States

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2:00 PM - TC02.02.02
Expanding Environmental Control with New Nanofluidic Platforms for Liquid Cell-(S)TEM

Trevor Moser 1 2 , Tolou Shokuhfar 3 , James Evans 1
1 , Pacific Northwest National Lab, Richland, Washington, United States, 2 , Michigan Technological University, Houghton, Michigan, United States, 3 , University of Illinois at Chicago, Chicago, Illinois, United States

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2:15 PM - TC02.02.03
In Situ Liquid Cell Localized Corrosion Involving Radiolysis in the Transmission Electron Microscope

Ainsley Pinkowitz 1 , David Duquette 1 , Robert Hull 1
1 , Rensselaer Polytechnic Institute, Troy, New York, United States

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2:30 PM - TC02.02.04
Quantitative Nanochemistry for Fundamental Understanding of Heterogeneous Nucleation

Mei Wang 1 , Taylor Woehl 1
1 , University of Maryland, College Park, Maryland, United States

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2:45 PM - TC02.02.05
In Situ Variable-Temperature Liquid Cell Transmission Electron Microscopy (VT-LCTEM) Study of Size-Stabilized Covalent Organic Framework (COF) Nanoparticle Nucleation and Growth

Lucas Parent 1 2 , Brian Smith 3 , Chiwoo Park 4 , Austin Evans 2 , William Dichtel 2 , Nathan Gianneschi 1 2
1 , University of California, San Diego, La Jolla, California, United States, 2 , Northwestern University, Evanston, Illinois, United States, 3 , Bucknell University, Rooke, Pennsylvania, United States, 4 , Florida State University, Tallahassee, Florida, United States

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3:00 PM -
BREAK

3:30 PM - *TC02.02.06
In Situ TEM Revealing of the Fundamental Physical and Chemical Process of Both Energy Storage and Nanoparticle System

Chongmin Wang 1
1 , Pacific Northwest National Laboratory, Richland, Washington, United States

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4:00 PM - TC02.02.07
In Situ Investigation of Nucleation, Growth, Corrosion Behavior in Atomic Layered Core-Shell Electocatalysts

Jianbo Wu 1 , Hao Shan 1 , Yanling Ma 1 , Fenglei Shi 1 , Tao Deng 1
1 , Shanghai Jiaotong University, Shanghai China

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4:15 PM - TC02.02.08
A Method to Measure of the Liquid Suspension Nanoparticle Size in Aerosols

Ja Young Park 1 , Min Jeong Kwak 1 , Nam woong Song 1
1 , Korea Research Institute of Standards and Science (KRISS), Daejeon Korea (the Republic of)

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4:30 PM - TC02.02.09
Characterization of Hydrothermally Synthesized Sodium-Yttrium-Fluoride Upconversion Nanocrystal

Xuezhe Zhou 1 , Guomin Zhu 1 2 , James De Yoreo 2 1 , Peter Pauzauskie 1 2
1 , University of Washington, Seattle, Washington, United States, 2 , Pacific Northwest National Laboratory, Richland, Washington, United States

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4:45 PM - TC02.02.10
In Situ Study of the Controlled Growth of Electron Beam-Induced Branch-Shaped Au Particles

Shih-Ting Wang 1 2 , Yiyang Lin 1 2 , Michael Nielsen 3 , Michael Thomas 1 2 , Chengyu Song 4 , Christopher Spicer 1 2 , Peter Ercius 4 , Shaul Aloni 4 , Molly Stevens 1 2
1 Materials, Imperial College London, London United Kingdom, 2 Bioengineering and Institute of Biomedical Engineering, Imperial College London, London United Kingdom, 3 Physical & Life Sciences Directorate, Lawrence Livermore National Laboratory, Berkeley, California, United States, 4 Molecular Foundry, Lawrence Berkeley National Laboratory, Berkeley, California, United States

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TC02.03: Poster Session I: In Situ—Study of Materials Transformation
Session Chairs
Daan Hein Alsem
Yuzi Liu
Monday PM, November 27, 2017
Hynes, Level 1, Hall B

8:00 PM - TC02.03.01
PtRu Nanoalloy Catalysts for Ethanol Oxidation Reaction—Experimental and Theoretical Assessments of Composition-Structure-Activity Correlation

Zhipeng Wu 1 2 , Emma Hopkins 1 , Keonwoo Park 1 , Yinguang Zhao 1 , Yazan Maswadeh 3 , Shiyao Shan 1 , Hannah Cronk 1 , Zakiya Skeete 1 , Binay Prasai 3 , Jin Luo 1 , Valeri Petkov 3 , Lichang Wang 2 4 , Chuan-Jian Zhong 1
1 Chemistry, State University of New York at Binghamton, Binghamton, New York, United States, 2 Key Laboratory for Green Chemical Technology of Ministry of Education, R&D Center for Petrochemical Technology, Tianjin University, Tianjin China, 3 Physics, Central Michigan University, Mt. Pleasant, Michigan, United States, 4 Chemistry, Southern Illinois University, Carbondale, Illinois, United States

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8:00 PM - TC02.03.02
Determination of Reaction Mechanism within Single Particle Layered Oxide Materials for Li-Ion Batteries Using Operando Diffraction Mapping

Brian May 1 , Mark Wolfman 1 2 , Kamila Wiaderek 2 , Olaf Borkiewicz 2 , Ruqing Xu 2 , Nicholas Faenza 3 , Nathalie Pereira 3 , Glenn Amatucci 3 , Peter Chupas 2 , Karena Chapman 2 , Jordi Cabana 1
1 Department of Chemistry, University of Illinois at Chicago, Chicago, Illinois, United States, 2 X-ray Science Division, Argonne National Laboratory, Argonne, Illinois, United States, 3 Department of Materials Science and Engineering, Rutgers, The State University of New Jersey, North Brunswick, New Jersey, United States

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8:00 PM - TC02.03.03
Comparison of the Growth of Metallic Silver Filaments in Ag2WO4 Samples by Means of Electron Beam and Ultraviolet Irradiation

Santiago Maya Johnson 1 , Julio Sczancoski 1 , Wyllamanney da Silva Pereira 1 , Elson Longo 1 , Edson Leite 1
1 , Federal University of Sao Carlos, Sao Carlos, SP, Brazil

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8:00 PM - TC02.03.04
Size-Dependent Depression of the Glass Transition Temperature in a Freestanding Polymer Nanofiber

Wuseok Kim 1 , Sangmin Jeon 1
1 , POSTECH, Pohang Korea (the Republic of)

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8:00 PM - TC02.03.05
Microstructural Characterization of an α+β type Ti-5.5Mo-7.2Al-4.5Zr-2.6Sn-2.1Cr Alloy During Recrystallization Annealing

Ran Shi 1 , Guoju Li 1 , Yumeng Xia 1 , Qunbo Fan 1 , Fuchi Wang 1 , Hongmei Zhang 1 , Xingwang Cheng 1
1 , Beijing Institute of Technology, Beijing China

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8:00 PM - TC02.03.06
TEM Specimen Preparation for In Situ Heating Experiments Using FIB

Sriram Vijayan 1 , Joerg Jinschek 2 3 , Stephan Kujawa 3 , Jens Greiser 3 , Mark Aindow 1
1 , University of Connecticut, Storrs, Connecticut, United States, 2 , The Ohio State University, Columbus, Ohio, United States, 3 , FEI Company, Achtseweg Noord 5, Eindhoven Netherlands

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8:00 PM - TC02.03.07
Probing Local Structural Changes Using In Situ Indentation and Raman Spectroscopy

Praveena Manimunda 1 , Manish Kumar Mishra 2 , S. A. Syed Asif 1
1 , Bruker Nano Surfaces, Eden Prairie, Minnesota, United States, 2 Department of Chemistry, The University of Alabama, Tuscaloosa, Alabama, United States

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8:00 PM - TC02.03.08
Elastic Properties of an Epoxy Resin Polymer During Structural Reconstitution

Manon Heili 1 , Andrew Bielawski 1 , John Kieffer 1
1 , Univ of Michigan, Ann Arbor, Michigan, United States

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8:00 PM - TC02.03.09
High-Resolution X-Ray Computed Tomography and Direct Numerical Simulation for the Measurement and Calculation of Decreased Permeability in the Wall-Flow Diesel Particulate Filter due to the Accumulation of Lubricant-Derived Ash

Carl Kamp 1 , Shawn Zhang 2 , Greg Monahan 2 , Sujay Bagi 1 , Yujun Wang 3
1 , Massachusetts Institute of Technology, Cambridge, Massachusetts, United States, 2 , DigiM Solution LLC, Burlington, Massachusetts, United States, 3 , Cummins, Columbus, Indiana, United States

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8:00 PM - TC02.03.10
On the Use of SEM Correlative Tools for In Situ Mechanical Tests

Qiwei Shi 1 , Stephane Roux 1 , Francois Hild 1 , Felix Latourte 2
1 , LMT, Cachan France, 2 MMC, EDF RD, Ecuelles France

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2017-11-28   Show All Abstracts

Symposium Organizers

Yuzi Liu, Argonne National Laboratory
Daan Hein Alsem, Hummingbird Scientific, Inc
Yugang Sun, Temple University
Lin Wang, Center for High Pressure Science and Technology Advanced Research

Symposium Support

Direct Electron, LP
Gatan, Inc.
TC02.04: Gas TEM
Session Chairs
Yuzi Liu
Scott Mao
Haimei Zheng
Tuesday AM, November 28, 2017
Hynes, Level 2, Room 200

8:30 AM - TC02.04.01
In Situ TEM Observation of Stress-Induced Spontaneous Growth of Oxide Nanocrystals in Ambient Cell

Chun-Cheng Chen 1 , Pai-Jui Hsu 1 , Shou-Yi Chang 1
1 , National Tsing Hua University, Hsinchu Taiwan

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8:45 AM - TC02.04.02
In Situ Observation of the Surface of Working Gold Electrodes by Environmental TEM

Ryotaro Aso 1 , Yohei Ogawa 1 , Hideto Yoshida 1 , Seiji Takeda 1
1 , The Institute of Scientific and Industrial Research, Osaka University, Osaka Japan

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9:00 AM - *TC02.04.03
In Situ High-Resolution TEM Study on Metal/Oxide Catalysts under Gas Environment

Ze Zhang 1 , Yong Wang 1
1 Center of Electron Microscopy, School of Materials Science and Engineering and State Key Laboratory of Silicon Materials, Zhejiang University, Hangzhou China

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9:30 AM - TC02.04.04
Understanding the Effects of Shape and Surface Faceting in the Hydrogenation Kinetics of Palladium Nanoparticles

Katherine Sytwu 1 , Fariah Hayee 1 , Tarun Narayan 1 , Ai Leen Koh 1 , Robert Sinclair 1 , Jennifer Dionne 1
1 , Stanford University, Stanford, California, United States

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9:45 AM - TC02.04.05
In Situ Characterization of Catalytic Reactions Promoted by Localized Surface Plasmon Resonance Energy

Canhui Wang 1 2 , Wei-Chang Yang 1 2 , Devika Sil 1 2 , Amit Agrawal 1 2 , Renu Sharma 1
1 , National Institute of Standards and Technology, Gaithersburg, Maryland, United States, 2 , University of Maryland, College Park, Maryland, United States

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10:00 AM -
BREAK

10:30 AM - *TC02.04.06
Environmental TEM of Crystal Growth and Epitaxy on Graphene

Frances Ross 1
1 , IBM T.J. Watson Research Center, Yorktown Heights, New York, United States

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11:00 AM - *TC02.04.07
In Situ Transmission Electron Microscopy with Atomic Resolution at Atmospheric Pressures

Xiaoqing Pan 2 1 , Sheng Dai 2 , George Graham 2 3
2 Chemical Engineering and Materials Science, University of California, Irvine, Irvine, California, United States, 1 Physics and Astronomy, University of California, Irvine, Irvine, California, United States, 3 Materials Science and Engineering, University of Michigan–Ann Arbor, Ann Arbor, Michigan, United States

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11:30 AM - TC02.04.08
Electron Energy Loss Spectroscopy Videos During In Situ Experiments

Benjamin Miller 1 , Stephen Mick 1
1 , Gatan, Inc., Pleasanton, California, United States

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11:45 AM - TC02.04.09
Forming Silicides and Germanides in Vertical Semiconductor Nanowires

Yi-Chia Chou 1 , Federico Panciera 2 , Mark Reuter 3 , Dmitri Zakharov 4 , Eric Stach 4 , Frances Ross 3
1 , National Chiao Tung University, Hsinchu Taiwan, 2 Department of Biological Sciences, National University of Singapore, Singapore Singapore, 3 , IBM T.J. Watson Research Center, Yorktown Heights, New York, United States, 4 , Brookhaven National Laboratory, Upton, New York, United States

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TC02.05: In Situ TEM for Energy Materials
Session Chairs
Amanda Petford-Long
Chongmin Wang
Tuesday PM, November 28, 2017
Hynes, Level 2, Room 200

2:00 PM - *TC02.05.02
In Situ TEM Studies of Energy Storage Mechanisms at Atomic Scales

Reza Shahbazian-Yassar 1
1 , University of Illinois at Chicago, Chicago, Illinois, United States

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2:30 PM - TC02.05.03
In Situ Observation of the Electrochemical Deposition of Iron in a Transmission Electron Microscope

Ulrike Wolff 1 , Bojan Ambrozič 2 , Janez Zavašnik 2 , Kristina Zuzek Rozman 2 , Karin Leistner 1 , Kornelius Nielsch 1 , Sašo Šturm 2
1 , IFW Dresden, Dresden Germany, 2 Department for Nanostructured Materials, Jozef Stefan Institute, Ljubljana Slovenia

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2:45 PM - TC02.05.04
In Situ Scanning Electron Microscope Observations of the Nucleation and Growth of Li Metal on Oxide Solid Electrolytes

Munekazu Motoyama 1 , Yuki Tanaka 1 , Takayuki Yamamoto 1 , Yasutoshi Iriyama 1
1 , Nagoya University, Nagoya Japan

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3:00 PM -
BREAK

3:30 PM - TC02.05.05
In Situ Investigation of Nano-to-Macroscale Reaction Pathways in Sulfide Materials for Alkali-Ion Batteries

Matthew McDowell 1 , Matthew Boebinger 1 , Francisco Quintero Cortes 1 , Neha Kondekar 1 , Michael Xu 1
1 , Georgia Institute of Technology, Atlanta, Georgia, United States

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TC02.06: Self-Assembly
Session Chairs
Yugang Sun
Tuesday PM, November 28, 2017
Hynes, Level 2, Room 200

3:45 PM - *TC02.06.01
Peering into the Self- and Directed-Assembly of Nanoparticles

Hongyou Fan 1 2
1 , Sandia National Laboratories, Albuquerque, New Mexico, United States, 2 , University of New Mexico, Albuquerque, New Mexico, United States

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4:15 PM - TC02.06.02
Label Free In Situ Three-Dimensional Monitoring of Nanoparticle Self-Assembly Processes

Benjamin Hogan 1 , Tatiana Perova 2 3 , Yuri Gun'ko 3 4 , Sergey Dyakov 5 , Monica Craciun 1 , Anna Baldycheva 1
1 College of Engineering, Mathematics and Physical Sciences, University of Exeter, Exeter United Kingdom, 2 Department of Electronic and Electrical Engineering, Trinity College Dublin, The University of Dublin, Dublin Ireland, 3 , ITMO University, St Petersburg Russian Federation, 4 School of Chemistry, Trinity College Dublin, The University of Dublin, Dublin Ireland, 5 Photonics and Quantum Material Center, Skolkovo Institute of Science and Technology, Moscow Russian Federation

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4:30 PM - TC02.06.03
Ion Induced Polymer Reflow for In Situ Self-Assembly of Three-Dimensional Nanostructures

Chunhui Dai 1 , Jeong-Hyun Cho 1
1 , University of Minnesota, Minneapolis, Minnesota, United States

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4:45 PM - TC02.06.04
In Situ GISAXS Analysis of Ligand Exchange on Quantum Dots Superlattice Films

Yaoting Wu 1 , Blaise Fleury 1 , Christopher Murray 1
1 , University of Pennsylvania, Philadelphia, Pennsylvania, United States

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TC02.07: Poster Session II: In Situ—Study of Materials Transformation
Session Chairs
Yuzi Liu
Yugang Sun
Lin Wang
Tuesday PM, November 28, 2017
Hynes, Level 1, Hall B

8:00 PM - TC02.07.01
Geometric Characterization of SWCNT-Induced Crystalline Growth in an Amorphous All-Aromatic Poly(ether imide)

Samuel Heroy 1 , Feng Shi 1 , Peter Mucha 1 , Theo Dingemans 1 , Greg Forest 1
1 , University of North Carolina at Chapel Hill, Chapel Hill, North Carolina, United States

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8:00 PM - TC02.07.02
Benchmarking Equations of State from DFT across the Materials Project for Computational Discovery

Katherine Latimer 2 , Kiran Mathew 1 , Shyam Dwaraknath 1 , Kristin Persson 1 2
2 Material Science, University of California, Berkeley, California, United States, 1 , Lawrence Berkeley National Laboratory, Berkeley, California, United States

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8:00 PM - TC02.07.03
In Situ Exploration of the Growth Mechanism of ZnO Nanostructures Using Liquid Cell Electron Microscopy

Yubo Wang 1 , Xing Lu 1 , Shuai Wang 1
1 School of Chemistry and Chemical Engineering, School of Materials Science and Engineering, Huazhong University of Science and Technology, Wuhan China

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8:00 PM - TC02.07.04
Capturing Solid Solutions During a First-Order Phase Transition of Li1+XMn2O4

Bohang Song 1 , Gabriel Veith 1 , Pamela Whitfield 1 , Melanie Kirkham 1 , Jue Liu 1 , Robert Schmidt 1 , Ashfia Huq 1
1 , Oak Ridge National Laboratory, Oak Ridge, Tennessee, United States

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8:00 PM - TC02.07.05
In Situ Synchrotron Study of Ferroelectric and High-κ Phase Formation in ALD Hafnium Oxide (HfO2) during Annealing

Vijay Narasimhan 1 , Stephen Weeks 1 , Donata Passarello 2 , Apurva Mehta 2 , Michael Toney 2 , Karl Littau 1 , Tony Chiang 1
1 , Intermolecular Inc., San Jose, California, United States, 2 , Stanford Synchrotron Radiation Lightsource, Menlo Park, California, United States

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8:00 PM - TC02.07.06
In Situ Measurement of Surface Relief Induced by Ferrite Plate Formation in a Low Carbon Steel by Digital Holographic Microscope

Shuhei Komine 1 , Junya Inoue 1 , Kenji Sekido 1
1 , The University of Tokyo, Meguro-ku Japan

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8:00 PM - TC02.07.07
In Situ X-Ray Diffraction Studies of Crystallization Growth Behavior in ZnO-Bi2O3-B2O3 Glass as a Route to Functional Optical Devices

Quentin Altemose 1 , Katie Raichle 1 , Brittani Schnable 1 , Casey Schwarz 1 , Myungkoo Kang 2 , Carlo Pantano 3 , Kathleen Richardson 2 , Clara Rivero-Baleine 4 , Stephen Kuebler 5 2 6
1 , Ursinus College, Collegeville, Pennsylvania, United States, 2 CREOL, The College of Optics & Photonics, University of Central Florida, Orlando, Florida, United States, 3 Materials Science and Engineering, Pennsylvania State University, State College, Pennsylvania, United States, 4 , Lockheed Martin, Orlando, Florida, United States, 5 Chemistry, University of Central Florida, Orlando, Florida, United States, 6 Physics, University of Central Florida, Orlando, Florida, United States

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8:00 PM - TC02.07.08
In Situ Electrochemical Observations of Si-Nanoparticles

Oskar Ronan 2 , Lorcan McKeon 1 , João Coelho 2 , Edmund Long 1 , Valeria Nicolosi 2
2 Chemistry, Trinity College Dublin, Dublin Ireland, 1 Physics, Trinity College Dublin, Dublin Ireland

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8:00 PM - TC02.07.09
In Situ Observation of Atomic Movement in Ferroelectric Thin Film under External Electric Field and Stress

Hyeon Jun Lee 1 , Erjia Guo 2 , Kathrin Dorr 3 , Jaekwang Lee 4 , Ji Young Jo 1
1 , Gwangju Institute of Science and Technology, Gwanju Korea (the Republic of), 2 , Oak Ridge National Laboratory, Oakridge, Tennessee, United States, 3 , Martin-Luther-University, Halle Germany, 4 , Pusan University, Pusan Korea (the Republic of)

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8:00 PM - TC02.07.10
Express-Method for the Study of Electrolyte Anion Profiles in the Bulk of Dense Anodic Alumina Films

Valentina Yakovtseva 1 , Dimitri Shimanovich 1 , Vitali Sokol 1 , Alexei Subko 1 , Vitaly Bondarenko 2
1 Micro- and Nanoelectronics, Belarusian State University of Informatics and Radioelectronics, Minsk Belarus, 2 Micro- and Nanoelectronics, Belarusian State University of Informatics and Radioelectronics, Minsk Belarus

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8:00 PM - TC02.07.11
New In Situ, Thermal Radiation, and Stray Light-Immune Stress and Thick Layer Metrology for Research and Production of Novel Materials

Wojciech Walecki 1 , John Groot 1
1 Research and Development, Frontier Semiconductors, San Jose, California, United States

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8:00 PM - TC02.07.12
Investigations into Pressure-Induced Magnetic and Structural Transitions in Magnetite (Fe3O4) Nanoparticles

Kalpani Werellapatha 1 , Carlos Escanhoela 2 3 , Daniel Haskel 2 , Robert Meulenberg 1 , Changyong Park 4
1 Department of Physics, University of Maine, Orono, Maine, United States, 2 Advanced Photon Source, Argonne National Laboratory, Argonne, Illinois, United States, 3 , Brazilian Synchrotron Light Laboratory (LNLS), Campinas Brazil, 4 , HPCAT, Geophysical Laboratory, Carnegie Institution of Washington, Argonne, Illinois, United States

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8:00 PM - TC02.07.13
Tracking Thermal Phase Transformations of Luminescence Materials with In Situ TEM

Xuezhe Zhou 2 , Julio Rodriguez Manzo 1 , Matthew Lim 2 , Norman Salmon 1 , Peter Pauzauskie 2
2 , University of Washington , Seattle, Washington, United States, 1 , Hummingbird Scientific, Lacey, Washington, United States

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8:00 PM - TC02.07.15
Rapid Feedback of Laser Assisted Chemical Vapor Deposition Growth Mechanisms by Operando X-Ray Diagnostics

Anthony Van Buuren 1 , Aiden Martin 1 , Philip Depond 1 , Michael Bagge-Hansen 1 , Jonathan Lee 1 , Jae-Hyuck Yoo 1 , Selim Elhadj 1 , Manyalibo Matthews 1
1 , Lawrence Livermore National Lab, Livermore, California, United States

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2017-11-29   Show All Abstracts

Symposium Organizers

Yuzi Liu, Argonne National Laboratory
Daan Hein Alsem, Hummingbird Scientific, Inc
Yugang Sun, Temple University
Lin Wang, Center for High Pressure Science and Technology Advanced Research

Symposium Support

Direct Electron, LP
Gatan, Inc.
TC02.08: In Situ X-Ray for Materials Science
Session Chairs
Michael Behr
Yang Ren
Lin Wang
Wednesday AM, November 29, 2017
Hynes, Level 2, Room 200

8:00 AM - TC02.08.01
Molecular Engineering of Nano-Optomechanical Transducers

Jacqueline Cole 1 2 3
1 , University of Cambridge, Cambridge United Kingdom, 2 , STFC Rutherford Appleton Laboratory, Harwell United Kingdom, 3 , Argonne National Laboratory, Chicago, Illinois, United States

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8:15 AM - TC02.08.02
In Situ X-Ray Phase Contrast Imaging of Rapid Phase Transformations and Violent Microexplosions During Combustion of Al:Zr Nanocomposite Powders

Elliot Wainwright 1 , Shashank Vummidi Lakshman 1 , Andrew Leong 1 , Alex Kinsey 1 , John Gibbins 1 , Shane Arlington 1 , Tao Sun 2 , Kamel Fezzaa 2 , Todd Hufnagel 1 , Timothy Weihs 1
1 , Johns Hopkins University, Baltimore, Maryland, United States, 2 Advanced Photon Source, Sector 32, Argonne National Laboratory, Lemont, Illinois, United States

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8:30 AM - *TC02.08.03
In Situ X-Ray Diffraction Studies on the Effect of Ferroelectricity During the Growth of Ferroelectric Multilayers

Matthew Dawber 1 , Rui Liu 1 , Benjamin Bein 1 , Hsiang-Chun Hsing 1 , Giulia Bertino 1 , Anna Gura 1 , Amanda Lai 1 , Kenneth Evans-Lutterodt 2 , Jeffrey Ulbrandt 3 , Randall Headrick 3
1 , Stony Brook University, Stony Brook, New York, United States, 2 , Brookhaven National Laboratory, Upton, New York, United States, 3 , The University of Vermont, Burlington, Vermont, United States

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9:00 AM - *TC02.08.04
In Situ X-Ray Analysis of Interfacial Processes

Michael Bedzyk 1 , Zhenxing Feng 2 , Bor-Rong Chen 1 , Martin McBriarty 1
1 , Northwestern University, Evanston, Illinois, United States, 2 , Oregon State University, Corvallis, Oregon, United States

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9:30 AM - TC02.08.05
An In Situ Study of the Perovskite to Brownmillerite Phase Transition Using a Novel Time-Resolved X-Ray Reflectivity Technique

Howie Joress 1 2 , Joel Brock 1 3 , Arthur Woll 1
1 Cornell High Energy Synchrotron Source, Cornell University, Ithaca, New York, United States, 2 Materials Science and Engineering, Cornell University, Ithaca, New York, United States, 3 School of Applied and Engineering Physics, Cornell University, Ithaca, New York, United States

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9:45 AM - TC02.08.06
Understand the Formation of Metal Nanoparticles with In Situ XRD and Ab Initio Computation

Xuetian Ma 1 , Jianming Bai 2 , Wenqian Xu 3 , Yifei Mo 4 , Hailong Chen 1
1 Mechanical Engineering, Georgia Institute of Technology, Atlanta, Georgia, United States, 2 National Synchrotron Light Source, Brookhaven National Laboratory, Upton, New York, United States, 3 Advanced Photon Source, Argonne National Laboratory, Lemont, Illinois, United States, 4 Materials Science and Engineering, University of Maryland, College Park, Maryland, United States

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10:00 AM -
BREAK

10:30 AM - *TC02.08.07
Coherent X-Ray Diffractive Imaging

Jianwei Miao 1
1 Department of Physics & Astronomy and California NanoSystems Institute, University of California, Los Angeles, Los Angeles, California, United States

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11:00 AM - TC02.08.08
Transcrystallization and Orientation in Polypropylene/Graphene Filaments in Additive Manufacturing

Yuval Shmueli 1 , Jiaolong Jiang 1 , Taejin Kim 1 , Ellen Wachtel 2 , Gad Marom 3 , Dilip Gersappe 1 , Miriam Rafailovich 1
1 , Stony Brook University, Stony Brook, New York, United States, 2 , Weizmann Institute of Science, Rehovot Israel, 3 , The Hebrew University of Jerusalem, Jerusalem Israel

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11:15 AM - TC02.08.09
High-Speed Synchrotron Imaging for Additive Manufacturing of Titanium Alloys

Andrew Kiss 1 , Anthony Fong 1 , Vivek Thampy 1 , Kevin Stone 1 , Christopher Tassone 1 , Nicholas Calta 2 , Philip Depond 2 , Jennifer Wang 2 , Aiden Martin 2 , Ryan Ott 3 , Manyalibo Matthews 2 , Anthony Van Buuren 2 , Michael Toney 1 , Johanna Weker 1
1 , SLAC National Accelerator Laboratory, Menlo Park, California, United States, 2 , Lawrence Livermore National Laboratory, Livermore, California, United States, 3 , Ames Laboratory, Ames, Iowa, United States

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11:30 AM - TC02.08.10
Evolution of Carbon Fiber Microstructure During High-Temperature Graphitization Measured In Situ Using Synchrotron Wide-Angle X-Ray Diffraction

Michael Behr 1 , James Rix 2 , Brian Landes 1 , Bryan Barton 1 , Eric Hukkanen 1 , Jasson Patton 1 , Steven Weigand 2 , Denis Keane 2
1 , The Dow Chemical Company, Midland, Michigan, United States, 2 , Northwestern University, Argonne, Illinois, United States

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11:45 AM - TC02.08.11
Elucidating Reaction Pathways in the Synthesis of Block Copolymer-Derived Gyroidal Mesoporous Superconductors via In Situ SAXS/WAXS and XAS

Peter Beaucage 1 , Francis DiSalvo 1 , Sol Gruner 1 , Ulrich Wiesner 1
1 , Cornell University, Ithaca, New York, United States

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TC02.09: 3D in High Speed
Session Chairs
Jianwei Miao
Lin Wang
Wednesday PM, November 29, 2017
Hynes, Level 2, Room 200

1:30 PM - *TC02.09.01
Interrogation of Multi-Element and Multi-Valence Material Evolution in In Situ Environmental TEM

Huolin Xin 1
1 Center for Functional Nanomaterials, Brookhaven National Laboratory, Upton, New York, United States

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2:00 PM - TC02.09.02
Time-Resolved 3D Structures of Individual Nanoparticles in Solution

Byung Hyo Kim 1 , Junyoung Heo 1 , Peter Ercius 2 , Hans Elmlund 3 , Jungwon Park 1
1 , Seoul National University, Seoul Korea (the Republic of), 2 , Lawrence Berkeley National Laboratory, Berkeley, California, United States, 3 , Monash University, Clayton, Victoria, Australia

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2:15 PM - TC02.09.04
Visualization of Kirkendall Void Evolution in Ni-Based Wires via In Situ X-Ray Tomography

Arun Bhattacharjee 1 , Aaron Yost 2 , Dinc Erdeniz 2 , David Dunand 2 , Ashley Paz y Puente 1
1 Mechanical and Materials Engineering, University of Cincinnati, Cincinnati, Ohio, United States, 2 Materials Science and Engineering, Northwestern University, Evanston, Illinois, United States

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2:30 PM -
BREAK

TC02.10/TC06.14: Joint Session II: In Situ Mechanical Testing
Session Chairs
Wednesday PM, November 29, 2017
Hynes, Level 2, Room 210

3:30 PM - *TC02.10.01/TC06.14.01
Quantifying Dislocation Slip Transmission by In Situ Micromechanics

Christoph Kirchlechner 1 2
1 , Max-Planck-Institut für Eisenforschung, Duesseldorf Germany, 2 Materialphysik, University of Leoben, Leoben Austria

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4:00 PM - TC02.10.02/TC06.14.02
Use of In Situ TEM to Characterize the Deformation-Induced Martensitic Transformation in 304 Stainless Steel

Djamel Kaoumi 1
1 , North Carolina State University, Raleigh, North Carolina, United States

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4:15 PM - TC02.10.03/TC06.14.03
A Multiscale Study of Non-Linear Strain Path Changes in Mg AZ31B Using In Situ Neutron Powder Diffraction, Laue Microdiffraction and Acoustic Emission

Karl Sofinowski 1 2 , Jan Capek 3 , Tobias Panzner 1 , Steven Van Petegem 1 , Helena Van Swygenhoven-Moens 1 2
1 , Paul Scherrer Institute, Villigen Switzerland, 2 EDMX, École Polytechnique Fédérale de Lausanne, Lausanne Switzerland, 3 Physics of Materials, Charles University, Prague Czechia

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4:30 PM - TC02.10.04/TC06.14.04
High Rate Deformation Behavior of Marterials via Micron Scale Ballistic Experiments

Edwin Thomas 1
1 , Rice University, Houston, Texas, United States

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4:45 PM - TC02.10.05/TC06.14.05
Imaging Strain Fields by Ptychographic Topography

Steven Van Petegem 1 , Ana Diaz 1 , Maxime Dupraz 1
1 , Paul Scherrer Institute, Villigen PSI Switzerland

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TC02.11: Poster Session III: In Situ—Study of Materials Transformation
Session Chairs
Daan Hein Alsem
Lin Wang
Wednesday PM, November 29, 2017
Hynes, Level 1, Hall B

8:00 PM - TC02.11.01
Characterizing PVA/Nanocellulose Composites and Their Water Swelling Using In Situ SAXS and WAXS

Jonathan Torstensen 1 , Spontak Richard 2 , Justin Ryan 2 , Kristin Syverud 3 1 , Soo Ah Jin 2 , Dag Breiby 1
1 , NTNU, Trondheim Norway, 2 , North Carolina State University, Raleigh, North Carolina, United States, 3 , The Paper and Fibre Research Institute, Trondheim Norway

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8:00 PM - TC02.11.04
Volmer-Weber Growth Observed by High Resolution Stress Measurement

Sergey Grachev 1 , Quentin Hérault 1 , Jun Wang 1 , Iryna Gozhyk 1 , Rémi Lazzari 2
1 Surface du verre et interfaces, Saint-Gobain Recherche, Aubervilliers France, 2 , Institut des Nanosciences de Paris, Paris France

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8:00 PM - TC02.11.06
Environmental Nanocalorimeter Integrated with Scanning Electron Microscope

Feng Yi 1 , Ana Stevanovic 1 , William Osborn 1 , Andrei Kolmakov 1 , David LaVan 1
1 , National Institute of Standards and Technology, Gaithersburg, Maryland, United States

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8:00 PM - TC02.11.07
Piezoelectric Response Induced Phase Transition in Perovskite Thin Films

Hyeon Jun Lee 1 , Chan-Ho Yang 2 , Hiroshi Funakubo 3 , Ji Young Jo 1
1 , Gwangju Institute of Science and Technology, Gwanju Korea (the Republic of), 2 , KAIST, Dajeon Korea (the Republic of), 3 , Tokyo Institute of Technology, Tokyo Japan

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8:00 PM - TC02.11.08
Experimental Investigation on Structural Evolution of Amorphous Indium-Based Oxide Films During Annealing by In Situ XRD and EXAFS Measurements

Junjun Jia 1 , Shingo Yamamoto 1 , Toshihiro Okajima 2 , Yuzo Shigesato 1
1 , Aoyama Gakuin University, Kanagawa Japan, 2 , Kyushu Synchrotron Light Research Center, Tosu, , Saga, Japan

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8:00 PM - TC02.11.10
Temperature Calibration of a MEMS-Based Heating Holder Inside the TEM

Sriram Vijayan 1 , Mark Aindow 1
1 Department of Materials Science and Engineering, University of Connecticut, Storrs, Connecticut, United States

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8:00 PM - TC02.11.11
In Situ Characterization of Metal Alloy Powder Bed Fusion Processes Using High-Speed X-Ray and Optical Probes

Manyalibo Matthews 1 , Nicholas Calta 1 , Philip Depond 1 , Jennifer Wang 1 , Aiden Martin 1 , Gabe Guss 1 , Kevin Stone 2 , Johanna Weker 2 , Andrew Kiss 2 , Anthony Fong 2 , Vivek Thampy 2 , Christopher Tassone 2 , Saad Khairallah 1 , Wayne King 1 , Ryan Ott 3 , Matthew Kramer 3 , Anthony Van Buuren 1 , Michael Toney 2
1 , Lawrence Livermore National Laboratory, Livermore, California, United States, 2 , SLAC National Laboratory, Stanford, California, United States, 3 , Ames Laboratory, Ames, Ohio, United States

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8:00 PM - TC02.11.12
Pressure Conditioning Studies of Glassy Thermosets and Semi-Crystalline Thermoplastics

Brendan Ondra 1 , Alan Lesser 1
1 , Univ of Massachusetts-Amherst, Amherst, Massachusetts, United States

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8:00 PM - TC02.11.13
In Situ Characterization of Lithium Primary Batteries Using EIS and TXM

Abhi Raj 1 , Jeung Park 1 , Daniel Steingart 1
1 ACEE, Princeton University, Princeton, New Jersey, United States

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8:00 PM - TC02.11.14
X-Ray Interferometry/Tomography of 3D Printed Flame Retardants/ABS Structures

Leslie Butler 1 , Omoefe Kio 1 , Godfrey Mills 1 , Jonathan McCarney 2 , Kyungmin Ham 1
1 , Louisiana State University, Baton Rouge, Louisiana, United States, 2 Process Development Center, Albemarle Corporation, Baton Rouge, Louisiana, United States

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2017-11-30   Show All Abstracts

Symposium Organizers

Yuzi Liu, Argonne National Laboratory
Daan Hein Alsem, Hummingbird Scientific, Inc
Yugang Sun, Temple University
Lin Wang, Center for High Pressure Science and Technology Advanced Research

Symposium Support

Direct Electron, LP
Gatan, Inc.
TC02.12: High Pressure Physics and Chemistry
Session Chairs
Lin Wang
Thursday AM, November 30, 2017
Hynes, Level 2, Room 200

8:00 AM - *TC02.12.01
Novel Superhard sp3 Carbon Allotrope from Cold-Compressed C70 Peapods

Bingbing Liu 1 , Mingguang Yao 1 , Xigui Yang 1
1 State Key Lab of Superhard Materials, Jilin University, Changcun China

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8:30 AM - *TC02.12.02
Effects of Simultaneous Pressure and Temperature on the Stability of Si24

Brent Fultz 1 , Peter Ahnn 1 , Timothy Strobel 2
1 , California Institute of Technology, Pasadena, California, United States, 2 Carnegie Institution of Washington, Geophysical Laboratory, Washington D.C., District of Columbia, United States

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9:00 AM - TC02.12.03
Coupling between the Electrical Conductivity and Nanocrystalline Structures in a Single Nanowire under High Pressure

Sudeshna Samanta 1 , Mokwon Lee 2 , Deok-Soo Kim 2 , Lin Wang 1
1 , Center for High Pressure Science & Technology Advanced Research, Shanghai China, 2 Department of Industrial Engineering, Hanyang University, Seoul Korea (the Republic of)

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9:15 AM - TC02.12.04
Conductivity Transition of Endohedral Fullerene under High Pressure

Cuiying Pei 1 , Lin Wang 1
1 , Center for High Pressure Science and Technology Advanced Research, Shanghai China

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9:30 AM - *TC02.12.05
Hydrogen Storage and Transport Properties of TiZrNi Alloys under High Pressure

Jaeyong Kim 1 2 , Sanghwa Lee 2 , Wenge Yang 2 3 , Lin Wang 2 3
1 Department of Physics, Hanyang University, Seoul Korea (the Republic of), 2 , HYU-HPSTAR-CIS High Pressure Research Center, Seoul Korea (the Republic of), 3 , HPSTAR, Shanghai China

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10:00 AM -
BREAK

10:30 AM - TC02.12.06
Structural Evolution of A3BX4-Type Compounds under High Pressure

Yang Lu 1
1 , Center for High Pressure Science & Technology Advanced Research (HPSTAR), Shanghai China

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TC02.13: In Situ Neutron Scattering
Session Chairs
Yang Ren
Lin Wang
Thursday AM, November 30, 2017
Hynes, Level 2, Room 200

10:45 AM - TC02.13.01
Computational Design and Performance Predication of Creep-Resistant Ferritic Superalloys

Shao-Yu Wang 1 , P.K. Liaw 1 , David Dunand 2 , Gautam Ghosh 2 , Gian Song 3 , Sungil Baik 2
1 , The University of Tennessee, Knoxville, Tennessee, United States, 2 , Northwestern University, Evanston, Illinois, United States, 3 , Oak Ridge National Laboratory, Knoxville, Tennessee, United States

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11:00 AM - TC02.13.02
Metals under High-Pressure, High Temperature or During Plastic Deformation—In Situ Studies of Thermo-Mechanical Response by Neutron and Synchrotron Quantum Beams

Klaus-Dieter Liss 2 3 1
2 , Australian Nuclear Science and Technology Organisation, Lucas Heights, New South Wales, Australia, 3 School of Mechanical, Materials, Mechatronic and Biomedical Engineering, University of Wollongong, Wollongong, New South Wales, Australia, 1 , Guangdong Technion - Israel Institute of Technology (GTIIT), Shantou China

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11:15 AM - TC02.13.03
Study of Microstructure Evolution and Mechanical Properties by an In Situ Neutron Approach on NbTaTiV Refractory High-Entropy Alloys

Chanho Lee 1 , Gian Song 3 , Michael Gao 2 , Rui Feng 1 , Peiyong Chen 1 , Yan Chen 3 , Ke An 3 , Wei Guo 3 , Jonathan Poplawsky 3 , Song Li 4 , Alice Hu 4 , Hahn Choo 1 , P.K. Liaw 1
1 , University of Tennessee, Knoxville, Tennessee, United States, 3 , Oak Ridge National Laboratory, Knoxville, Tennessee, United States, 2 , National Energy Technology Laboratory, Albany, Oregon, United States, 4 , The City University of Hong Kong, Kowloon Hong Kong

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11:30 AM - *TC02.13.04
The Discovery of the Proton Polaron

Artur Braun 1
1 , Empa, Swiss Federal Laboratories for Materials Science and Technology, Duebendorf Switzerland

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TC02.14: In Situ X-Ray for Energy Materials
Session Chairs
Michael Bedzyk
Thursday PM, November 30, 2017
Hynes, Level 2, Room 200

1:30 PM - *TC02.14.01
Operando Electrochemical Scanning Transmission X-Ray Microscopy of Energy Conversion and Storage Electrode Materials

J. Tyler Mefford 1 2 , Jongwoo Lim 3 , Yiyang Li 1 , Norman Salmon 4 , William C. Chueh 1 2
1 Material Science and Engineering, Stanford University, Stanford, California, United States, 2 Stanford Institute for Materials & Energy Sciences, SLAC National Accelerator Laboratory, Menlo Park, California, United States, 3 Chemistry, Seoul National University, Seoul Korea (the Republic of), 4 , Hummingbird Scientific, Lacey, Washington, United States

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2:00 PM - TC02.14.02
High-Rate Operando Synchrotron X-Ray Diffraction and Spectroscopy of Non-Nanostructured Oxides for Energy Storage

Kent Griffith 1 , Clare Grey 1
1 Department of Chemistry, University of Cambridge, Cambridge United Kingdom

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2:15 PM - TC02.14.03
The Use of Ex Situ, In Situ, and Operando X-Ray Diffraction to Understand Rate-Dependent Phenomena in Energy Storage Materials and Systems

Alexander Brady 1 , Yiman Zhang 1 , Qing Zhang 1 , Christopher Pelliccione 2 , Haoyue Guo 1 , Paul Smith 1 , Ping Liu 2 , Andrea Bruck 1 , David Bock 2 , Jing Li 1 , Eric Stach 2 , Venkata Siva Varun Sarbada 3 , Robert Hull 3 , Esther Takeuchi 1 2 , Kenneth Takeuchi 1 , Amy Marschilok 1
1 , Stony Brook University, Stony Brook, New York, United States, 2 , Brookhaven National Laboratory, Upton, New York, United States, 3 , Rensselaer Polytechnic Institute, Troy, New York, United States

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2:30 PM - TC02.14.04
Operando Chemical Imaging of Ni-Based Layered Cathodes for Lithium-Ion Batteries

Mark Wolfman 1 , Young-Sang Yu 2 , Vincent De Andrade 3 , Antonin Grenier 3 , Hao Liu 3 , Kamila Wiaderek 3 , Olaf Borkiewicz 3 , Peter Chupas 3 , Karena Chapman 3 , Jordi Cabana 1
1 Department of Chemistry, University of Illinois Chicago, Chicago, Illinois, United States, 2 Advanced Light Source, Lawrence Berkeley National Laboratory, Berkeley, California, United States, 3 X-ray Science Division, Argonne National Laboratory, Lemont, Illinois, United States

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2:45 PM - TC02.14.05
Local Structural Fingerprint for Tracking Li-Ion Intercalation in Zero-Strain Lithium Titanate from In Situ X-Ray Absorption Spectroscopy and First-Principles Calculations

Mehmet Topsakal 1 , Wei Zhang 1 , Christina Cama 2 , Yimei Zhu 1 , Anatoly Frenkel 1 , Amy Marschilok 2 , Kenneth Takeuchi 2 , Esther Takeuchi 1 2 , Feng Wang 1 , Deyu Lu 1
1 , Brookhaven National Laboratory, Upton, New York, United States, 2 , Stony Brook University, Stony Brook, New York, United States

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3:00 PM -
BREAK

3:30 PM - TC02.14.06
A Multiscale (Molecular- to Meso-Scale) Approach for Understanding Electrochemical Energy Storage Systems—Opportunities and Insights via Advanced Characterization and Theory

Amy Marschilok 1 , Kenneth Takeuchi 1 , Esther Takeuchi 1 2
1 , Stony Brook University, Stony Brook, New York, United States, 2 , Brookhaven National Laboratory, Upton, New York, United States

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3:45 PM - TC02.14.07
In Situ Investigation into the Effects of Processing Conditions on Cation Mixing and Performance of an NMC 111 Cathode Material

Jeffrey Ovens 1 2 , Audrey Taylor 1 , Yingzi Feng 2 , Majid Talebi-Esfandarani 2 , Stephen Campbell 2 , Byron Gates 1
1 Chemistry, Simon Fraser University, Burnaby, British Columbia, Canada, 2 , Nano One Materials Corp., Burnaby, British Columbia, Canada

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4:00 PM - TC02.14.08
Graphene Liquid Cells Enable In Situ Spectro-Microscopies with Low Energy Electrons

Andrei Kolmakov 1
1 , National Institute of Standards and Technology, Gaithersburg, Maryland, United States

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4:15 PM - TC02.14.09
Multi-Modal Characterization of Metallic Nanocatalysts inside Fuel Cells by In Operando Energy Dispersive X-Ray Spectroscopy and Atomic Pair Distribution Analysis

Valeri Petkov 1
1 , Central Michigan University, Mt Pleasant, Michigan, United States

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4:30 PM - TC02.14.10
In Situ X-Ray Characterization of MnOx Polymorphs Formation Pathways via Hydrothermal Synthesis

Bor-Rong Chen 5 , Wenhao Sun 1 2 , Daniil Kitchaev 1 , Vivek Thampy 5 , Michael Toney 5 4 , Gerbrand Ceder 1 2 3 , Kevin Stone 5 , Laura Schelhas 5 4
5 Stanford Synchrotron Light Source, SLAC National Accelerator Laboratory, Menlo Park, California, United States, 1 Department of Materials Science and Engineering, Massachusetts Institute of Technology, Cambridge, Massachusetts, United States, 2 Materials Science Division, Lawrence Berkeley National Laboratory, Berkeley, California, United States, 4 Applied Energy Programs, SLAC National Accelerator Laboratory, Menlo Park, California, United States, 3 Department of Materials Science and Engineering, University of California, Berkeley, Berkeley, California, United States

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4:45 PM - TC02.14.11
In Situ Structural Characterization of Nanoalloy Catalysts for Low-Temperature Catalytic Oxidation of Hydrocarbons

Shiyao Shan 1 , Haval Kareem 1 , Jing Li 1 , Hannah Cronk 1 , Casey O'Brien 2 , Dat Tran 2 , Ivan Lee 2 , Valeri Petkov 3 , Jin Luo 1 , Chuan-Jian Zhong 1
1 Chemistry, State University of New York at Binghamton, Binghamton, New York, United States, 2 , U.S. Army Research Laboratory, Aldephi, Washington, United States, 3 Department of Physics, Central Michigan University, Mount Pleasant, Michigan, United States

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2017-12-01   Show All Abstracts

Symposium Organizers

Yuzi Liu, Argonne National Laboratory
Daan Hein Alsem, Hummingbird Scientific, Inc
Yugang Sun, Temple University
Lin Wang, Center for High Pressure Science and Technology Advanced Research

Symposium Support

Direct Electron, LP
Gatan, Inc.
TC02.15: Emerging Techniques
Session Chairs
Robert Bell
Yongsheng Han
Friday AM, December 01, 2017
Hynes, Level 2, Room 200

8:00 AM - *TC02.15.01
In Situ Studies of Crystallization and the Surrounding Effect

Yongsheng Han 1 , Tao Yang 1 , Kai Wang 1 , Jinghai Li 1
1 , Institute of Process Engineering, Chinese Academy of Science, Beijing China

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8:30 AM - TC02.15.02
Near-Real Time In Situ Analysis of Supported Nanoparticle Ensemble Evolution

Dmitri Zakharov 1 , Eric Stach 1 , Yuewei Lin 1 , Rémi Rémi Mégret 3 , Shinjae Yoo 1 , Peter Voorhees 2
1 , Brookhaven National Laboratory, Upton, New York, United States, 3 , University of Puerto Rico at Mayagüez, Mayagüez, Puerto Rico, United States, 2 Department of Materials Science and Engineering, Northwestern University, Evanston, Illinois, United States

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8:45 AM - TC02.15.03
In Situ Liquid Cell Capabilities for Helium Ion Microscopy to Visualize Organic Compounds in Their Native Environments

Alison Pawlicki 1 2 , Matthew Burch 2 , Raymond Unocic 2 , Jeff Fowler 3 , Songkil Kim 2 , Anton Ievlev 2 , Alex Belianinov 2 , Olga Ovchinnikova 2
1 The Bredesen Center, University of Tennessee, Oak Ridge, Tennessee, United States, 2 Center for Nanophase Materials Sciences and Institute for Functional Imaging of Materials, Oak Ridge National Laboratory, Oak Ridge, Tennessee, United States, 3 , Syngenta Crop Protection, Greensboro, North Carolina, United States

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9:00 AM - TC02.15.04
In Situ Electron Channeling Microscopy of Recombination-Enhanced Dislocation Motion in Heterogeneously-Integrated GaAs on Si for Quantum Dot Lasers

Patrick Callahan 1 , Daehwan Jung 1 , Gareth Seward 1 , John Bowers 1 , Kunal Mukherjee 1
1 , University of California, Santa Barbara, Santa Barbara, California, United States

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9:15 AM - TC02.15.05
In Situ Surface Structure of Bimetallic Nanoporous Catalysts—The Effect of Nanoscale Flow

Matthew Montemore 1 , Andrea Montessori 2 , Sauro Succi 1 2 , Cedric Barroo 1 , Giacomo Falcucci 2 1 , David Bell 1 , Efthimios Kaxiras 1
1 , Harvard University, Cambridge, Massachusetts, United States, 2 , University of Rome, Rome Italy

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9:30 AM - TC02.15.06
Atom by Atom Fabrication via Beam Controlled Organic Reactions

Ondrej Dyck 1 , Sergei Kalinin 1 , Artem Maksov 2 , Stephen Jesse 1
1 , Oak Ridge National Lab, Oak Ridge, Tennessee, United States, 2 , University of Tennessee, Knoxville, Knoxville, Tennessee, United States

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9:45 AM -
BREAK

10:15 AM - TC02.15.07
Electrical Annealing of Metal Microstructures

Baoming Wang 1 , Daudi Warywoba 2 , MD Zahabul Islam 1 , Aman Haque 1
1 , The Pennsylvania State University, State College, Pennsylvania, United States, 2 , The Pennsylvania State University, DuBois, Pennsylvania, United States

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10:30 AM - TC02.15.08
Development of and Initial Results from the First In Situ Ion Irradiation Dynamic TEM

Patrick Price 1 , Michael Abere 1 , Christopher Barr 1 , Sang Park 2 , Bryan Reed 2 , Daniel Masiel 2 , David Adams 1 , Khalid Hattar 1 , Samuel Briggs 1
1 , Sandia National Laboratories, Albuquerque, New Mexico, United States, 2 , Integrated Dynamic Electron Solutions, Pleasanton, California, United States

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10:45 AM - TC02.15.09
Dynamic TEM Characterization of Unsteady Propagation During Laser Crystallization of Amorphous Germanium

Garth Egan 1 , Tian Li 1 , John Roehling 1 , Joseph McKeown 1 , Geoffrey Campbell 1
1 , Lawrence Livermore National Laboratory, Livermore, California, United States

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11:00 AM - TC02.15.10
In Situ Ion Irradiation on Al-Co-Cr-Fe-Ni High Entropy Alloys

Jing Hu 1 , Rui Feng 2 , P.K. Liaw 2 , Meimei Li 1 , Mark Kirk 1
1 , Argonne National Laboratory, Lemont, Illinois, United States, 2 , University of Tennessee, Knoxville, Tennessee, United States

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11:15 AM - TC02.15.11
High Throughput Screening of Metastable Phase Formation Applied to Compositions on Gradient between Computationally Predicted Piezoelectrics

Robert Bell 1
1 , Cornell University, Ithaca, New York, United States

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11:30 AM - TC02.15.12
Diagnosing CNT Growth Quality Using In Situ Ambient Pressure—X-Ray Photoelectron Spectroscopy

Jennifer Carpena 1 2 , J. Boscoboinik 3 4 , Sammy Saber 1 5 , Jianqiang Zhong 4 , Rahul Rao 1 5 , Matthew Maschmann 6 , Dmitri Zakharov 4 , Eric Stach 4 , Benji Maruyama 1
1 Materials and Manufacturing Directorate, Air Force Research Laboratory, WPAFB, Ohio, United States, 2 , National Research Council, Washington, District of Columbia, United States, 3 Center for Functional Nanomaterials, Brookhaven National Laboratory, Upton, New York, United States, 4 National Synchrotron Light Source II, Brookhaven National Laboratory, Upton, New York, United States, 5 , UES, Inc., Dayton, Ohio, United States, 6 , University of Missouri, Columbia, Missouri, United States

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11:45 AM - TC02.15.13
Analyzing Copper Etching Dynamics by Hybridizing AFM Controlled SECM with Raman microSpectroscopy

Yirmi Bernstein 1 , Yossi Bar-David 3 , Dmitry Lev 1 , Rimma Dechter 1 , Sofia Kokotov 2 , Oleg Fedosyeyev 2 , Aaron Lewis 1
1 Applied Physics, The Hebrew University of Jerusalem, Jer Israel, 3 Chemistry Department, The Hebrew University of Jerusalem, Jerusalem Israel, 2 , Nanonics Imaging, Jerusalem Israel

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