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 Volume 1243
Editors: Hector A. Calderon, Armando Salinas Rodriguez, Heberto Balmori-Ramírez, J.Gerardo Cabañas-Moreno, Kozo Ishizaki
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Editors: Boris E. Burakov and Albert S. Aloy
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 August 2008 -- Hard Materials with Tunable Porosity

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Editors: J. Wu, W. han, A. Janotti, H-C. Kim
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 Volume 1144
Editors: Y. Cui, E.P.A.M. Bakkers, L. Lauhon, A. Talin
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 Volume 1128
Editors: M. Palm, B.P. Bewlay, M. Takeyama, J.M.K. Wiezorek, Y-H. He
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 August 2007 -- Glasses: At the Cutting Edge of Metals Research

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• printer-friendly

Author(s):
Ram Seshadri, Serena Ann Corr, Daniel P Shoemaker

Routes to porous materials with nanoscale dimensions have been investigated. In the first example presented, porous manganese oxide has been prepared by leaching Ni metal from a nickel-manganese oxide precursor via reduction. Electron microscopy studies have revealed the presence of Ni nanoparticles on the surface, and also embedded within the porous MnO matrix. Magnetic measurements have shown exchange bias between the ferromagnetic Ni nanoparticles and the antiferromagnetic MnO phase. In the second system studied, porous nanostructures of rutile VO2 and corundum V2O3 have been prepared by reduction of amine-templated V2O5-δ nanoscrolls. The porosity of these materials has been probed by electron microscopy, N2 sorption measurements and thermogravimetric analysis.

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Track ID:
Paper #: 1148-PP10-01
DOI: 10.1557/PROC-1148-PP10-01