Meetings & Events

2013 MRS Spring Meeting Logo

2013 MRS Spring Meeting & Exhibit

April 1-5, 2013 | San Francisco
Meeting Chairs: Mark L. Brongersma, Vladimir Matias, Rachel Segalman, Lonnie D. Shea, Heiji Watanabe

Symposium J : In-Situ Characterization Methods in Energy Materials Research

2013-04-02   Show All Abstracts

Symposium Organizers

John D. Baniecki, Fujitsu Laboratories
Paul C. McIntyre, Stanford University
Gyula Eres, Oak Ridge National Laboratory
A. Alec Talin, National Institute of Standards and Technology
Andreas Klein, Technische Universitaet Darmstadt

Symposium Support

E.A. Fischione Instruments, Inc.
J3: Neutron and Synchrotron Radiation
Session Chairs
Paul C. McIntyre
Gyula Eres
Tuesday PM, April 02, 2013
Moscone West, Level 2, Room 2008

2:45 AM - *J3.01
``Operando" Studies on Li-ion Batteries Using Neutron and Synchrotron Radiation

Helmut Ehrenberg 1 2 6 Anatoliy Senyshyn 3 Oleksandr Dolotko 2 Martin J. Muehlbauer 2 Manuel Hinterstein 4 Markus Herklotz 5 Kristian Nikolowski 1 Michael Knapp 1 6

1Karlsruhe Institute of Technology (KIT) Eggenstein-Leopoldshafen Germany2Technische Universitaet Darmstadt Darmstadt Germany3Technische Universitaet Muenchen Garching Germany4Technische Universitaet Dresden Dresden Germany5IFW Dresden Dresden Germany6Helmholtz-Institute Ulm Karlsruhe Germany

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3:15 AM - J3.02
Electrochemical In-situ and Operando Analyses of Batteries, Ceramic Fuel Cells, Gas Sensors and Photo-electrochemical Cells during Soft and Hard X-Ray Spectroscopy and Neutron Scattering under Various Thermodynamic Parameters

Artur Braun 1

1Empa. Swiss Federal Laboratories for Materials Science and Technology Dubendorf Switzerland

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3:30 AM - J3.03
Inelastic Neutron Scattering (INS) Studies of Hydrogen Spillover on Pure and Pd Decorated Metal Oxides

Sourav Adak 1 L. L. Daemen 2 J. Olliver 3 T. Seydel 3 C. Sumner 4 J. Z. Larese 1

1University of Tennessee Knoxville USA2Los Alamos National Laboratory Los Alamos USA3Institut Laue-Langevin Grenoble France4Eastman Chemical Company Kingsport USA

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3:45 AM - J3
J3.04 Transferred to J7.07

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4:00 AM - J3
BREAK

J4: Scanning Probe and Electron Microscopies
Session Chairs
John D. Baniecki
Andreas Klein
Tuesday PM, April 02, 2013
Moscone West, Level 2, Room 2008

4:30 AM - J4.01
Nanometer-scale Mapping of Electrochemical Nucleation on Li-ion Electrolytes

Amit Kumar 1 Thomas M Arruda 1 Alexander Tselev 1 Jamie Lawton 2 Tom Zawodzinski 2 3 Stephen Jesse 1 Sergei V Kalinin 1

1Oak Ridge National Lab Oak Ridge USA2University of Tennessee Knoxville USA3Oak Ridge National Lab Knoxville USA

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4:45 AM - J4.02
Synergistic Effects Among Cellulases during Enzymatic Cellulose Degradation, Visualized by In situ Atomic Force Microscopy

Thomas Ganner 1 Patricia Bubner 3 Manuel Eibinger 3 Claudia Mayrhofer 2 Harald Plank 1 2 Bernd Nidetzky 3

1Graz University of Technology Graz Austria2Center for Electron Microscopy Graz Austria3Graz University of Technology Graz Austria

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5:00 AM - J4.03
Dynamics of Al-Li Alloy Formation in Al Anode of Thin Film Batteries

Marina S. Leite 1 2 Dmitry Ruzmetov 1 2 Zhipeng Li 3 Leonid Bendersky 3 Alabert Alec Talin 1 4

1NIST Gaithersburg USA2University of Maryland College Park USA3NIST Gaithersburg USA4Sandia National Laboratories Livermore USA

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5:15 AM - J4.04
Concurrent Mechanical Testing and Lithiation of Silicon Nanowires during Scanning Electron Microscopy

Steven Boles 1 Oliver Kraft 1 Reiner Moenig 1

1Karlsruhe Institute of Technology Eggenstein-Leopoldshafen Germany

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J1 :Electron Microscopy I
Session Chairs
Helmut Ehrenberg
John D. Baniecki
Tuesday AM, April 02, 2013
Moscone West, Level 2, Room 2008

9:15 AM - *J1.01
Platforms and Methods for In Situ Characterization of Li-ion Battery Materials Using High Spatial Resolution Transmission Electron/Transmission X-Ray Microscopies

John Sullivan 1 N. C. Bartelt 1 F. El Gabaly 1 K. Fenton 2 C. T. Harris 2 Y. Liu 2 K. McCarty 1 A. McDaniel 1 G. Nagasubramanian 2 M. Shaw 2 J. Sugar 1 A. Talin 1 K. Zavadil 2 W. Chueh 3 T. Tyliszczak 4

1Sandia National Labs Livermore USA2Sandia National Labs Albuquerque USA3Stanford University Stanford USA4Lawrence Berkeley National Lab Berkeley USA

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9:45 AM - J1.02
Studying Dynamic Processes Occurring in Gas/Fluid Environmental Cells by TEM/STEM/DTEM

Patricia Abellan 1 James E. Evans 2 Taylor J. Woehl 3 Pushkarraj V. Deshmukh 4 Katherine L. Jungjohann 3 Joseph T. McKeown 5 Shareghe Mehraeen 6 Lucas R. Parent 3 Pinghong Xu 3 Hao Yang 3 Ilke Arslan 1 William D. Ristenpart 3 7 Nigel D. Browning 1

1Pacific Northwest National Laboratory Richland USA2Pacific Northwest National Laboratory Richland USA3University of California Davis USA4E.A. Fischione Instruments Export USA5Lawrence Livermore National Laboratory Livermore USA6University of California Davis USA7University of California Davis USA

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10:00 AM - J1.03
Nanofluidic Cells with Controlled Path Length and Liquid Flow for Rapid, High-resolution In Situ Electron Microscopy

Christina Mueller 1 5 2 Maher Harb 5 Jason R. Dwyer 4 5 R.J. Dwayne Miller 3 1 2

1University of Toronto Toronto Canada2University of Toronto Toronto Canada3University of Hamburg Hamburg Germany4University of Rhode Island Kingston USA5Insight Nanofluidics Toronto Canada

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10:15 AM - J1.04
In Situ Transmission Electron Microscopy of Electrochemical Reaction in Liquids

Minghua Sun 1 Hong-gang Liao 1 Kaiyang Niu 1 Haimei Zheng 1

1Lawrence Berkeley National Lab Berkeley USA

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10:30 AM - J1.05
Towards Optimizing Synthesis of Metallic Nanostructures in Soft Templates Using in-situ Liquid Stage Microscopy

Lucas Parent 1 David Robinson 2 Patrick Cappillino 2 James Evans 3 Nigel Browning 1 3 Ilke Arslan 3

1University of California, Davis Davis USA2Sandia National Laboratories Livermore USA3Pacific Northwest National Laboratory Richland USA

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10:45 AM - J1.06
In-situ Observation of Galvanic Replacement Reaction in K-kit by Transmission Electron Microscopy

Yu-Ting Chen 1 Tri-Rung Yew 1

1National Tsing Hua University Hsinchu Taiwan

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11:00 AM - J1
BREAK

J2: Electron Microscopy II
Session Chairs
John Sullivan
Alec Talin
Tuesday AM, April 02, 2013
Moscone West, Level 2, Room 2008

11:30 AM - J2.01
Revealing Size-dependent Oxygen Adsorption Strength on Cobalt Nanocatalyts by In Situ Environmental TEM Observations in Reactive Conditions

Huolin L. Xin 1 Sophie Carenco 1 Arda Genc 2 Libor Kovarik 2 Chongmin Wang 2 Elzbieta Pach 1 Miquel Salmeron 1 Haimei Zheng 1

1Lawrence Berkeley National Lab Berkeley USA2Pacific Northwest National Laboratory Richland USA

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11:45 AM - J2.02
In-situ ETEM and XANES Studies of Manganite Pervoskite Electro-catalysts for Oxygen Evolution

Christian Jooss 1 Stephanie Raabe 1 Daniel Mierwaldt 1 Jim Ciston 3 Matthe Uijttewaal 4 Joerg Hoffmann 1 Peter Bloechl 4 1 Yimei Zhu 2

1University of Goettingen Goettingen Germany2Brookhaven National Laboratory Upton USA3Lawrence Berkeley National Laboratory Berkeley USA4Technical University of Clausthal Clausthal Germany

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12:00 PM - J2.03
In-situ Transmission Electron Microscopy Study of Electrochemical Lithiation and Delithiation Cycling of RuO2 Nanowires as Conversion Anodes

Yang Liu 2 Keith Gregorczyk 1 John Sullivan 3 Gary Rubloff 1

1University of Maryland College Park USA2Sandia National Laboratories Albuquerque USA3Sandia National Laboratories Livermore USA

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12:15 PM - J2.04
Combining Quantitative Electrochemistry and Electron Microscopy to Study Reversible Lithiation of Silicon Nanowires

Kevin R Zavadil 1 Yang Liu 1 C. Thomas Harris 1 John P Sullivan 2

1Sandia National Laboratories Albuquerque USA2Sandia National Laboratories Livermore USA

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12:30 PM - J2.05
Real-time TEM Observation of Nano-voids in Silicon Battery Electrodes: Insight into Engineering Strategies for Structure Stabilization

Khim Karki 1 Jeong-Hyun Cho 2 ChuanFu Sun 3 YuHuang Wang 3 Tom Picraux 2 John Cumings 1

1University of Maryland College Park USA2Los Alamos National Laboratory Los Alamos USA3University of Maryland College Park USA

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2013-04-03   Show All Abstracts

Symposium Organizers

John D. Baniecki, Fujitsu Laboratories
Paul C. McIntyre, Stanford University
Gyula Eres, Oak Ridge National Laboratory
A. Alec Talin, National Institute of Standards and Technology
Andreas Klein, Technische Universitaet Darmstadt

Symposium Support

E.A. Fischione Instruments, Inc.
J7: Electronic Structure and Transport
Session Chairs
Gyula Eres
Alec Talin
Wednesday PM, April 03, 2013
Moscone West, Level 2, Room 2008

2:30 AM - *J7.01
Electronic Properties of Energy Converting Electrochemical Interfaces: Perspectives and Limitations of Quasi In-situ Surface Science Experiments

Wolfram Jaegermann 1

1TU Darmstadt Darmstadt Germany

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3:00 AM - J7.02
In-situ Study of Initial Growth and Electronic Properties of Al2O3 on Transparent Conducting Oxides

Anne Fuchs 1 Thorsten Bayer 1 Wolfram Jaegermann 1 Andreas Klein 1

1Darmstadt University of Technology Darmstadt Germany

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3:15 AM - *J7.03
In-situ High Temperature Studies on Ultra-thin Oxides and Heterostructures for Electrochemical Energy

Shriram Ramanathan 1

1Harvard University Cambridge USA

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3:45 AM - J7
BREAK

4:00 AM - *J7.04
Interface Formation in Energy Materials: In Situ Spectroscopy Study of STO Surface and LAO/STO Interface

Milan Radovic 1 2

1EPF Lausanne Switzerland2Swiss Light Source, Paul Scherrer Institut Villigen PSI Switzerland

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4:30 AM - J7.05
In-Situ Characterization of Conduction-band Offsets Using X-Ray Photoemission Spectroscopy and Correlation to Thickness Dependent Thermoelectric Properties of SrTiO3/Sr1-xLaxTiO3 and SrZrO3/Sr1-xLaxTiO3 Heterostructures

John Baniecki 1 Masatoshi Ishii 1 Hiroyuki Aso 1 Kazuaki Kurihara 1 Robert Schafranek 2 Kian Kerman 3

1Fujitsu Laboratories Atsugi Japan2Laboratoire de l'Intamp;#233;gration du Matamp;#233;riau au Systamp;#232;me Bordeaux France3Harvard University Cambridge USA

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4:45 AM - J7.06
Self Terminating Two-Dimensional Platinum Electrodeposition

Dincer Gokcen 1 Yihua Liu 1 Ugo Bertocci 1 Thomas P. Moffat 1

1National Institute of Standards and Technology Gaithersburg USA

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5:00 AM - J7.07
In-situ Investigation of Oxygen Exchange in Solid Oxide Fuel Cells Cathode Materials

Lorenzo Malavasi 1 Alessandro Mancini 1

1University of Pavia and INSTM Pavia Italy

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J8: XRAY III (XAS)
Session Chairs
Wolfram Jaegermann
Andreas Klein
Wednesday PM, April 03, 2013
Moscone West, Level 2, Room 2008

5:15 AM - *J8.01
In-situ Characterization of the Thermal Degradation of LiNi0.8Co0.15Al0.05O2 Cathode Materials for Lithium Ion Batteries: Insights from Combined Synchrotron XRD, XAS and Environmental Microscopy Studies

Seong-Min Bak 1 2 4 Kyung-Wan Nam 1 Won-Young Chang 2 Xiqian Yu 1 Enyuan Hu 1 Soo-Yeon Hwang 3 Kwang Bum Kim 4 Kyung Yoon Chung 2 Xiao Qing Yang 1 Eric A. Stach 3

1Brookhaven National Laboratory Upton USA2Korea Institute of Science and Technology (KIST) Seoul Republic of Korea3Brookhaven National Laboratory Upton USA4Yonsei University Seoul Republic of Korea

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5:45 AM - J8.02
In-situ XAS Study of Self-switching Electrocatalyst for OER and ORR

Gregory S Hutchings 1 Feng Jiao 1

1University of Delaware Newark USA

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J9: Poster Session
Session Chairs
John D. Baniecki
Alec Talin
Wednesday PM, April 03, 2013
Marriott Marquis, Yerba Buena Level, Salons 7-8-9

9:00 AM - J9.01
Determination of Polarization Dependence of Schottky Barrier Heights at Ferroelectric/Electrode Interfaces

Feng Chen 1 Shunyi Li 1 Andreas Hubmann 1 Andreas Klein 1

1Darmstadt University of Technology Darmstadt Germany

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9:00 AM - J9.03
Using the Dynamics of Fluorescent Cations to Probe and Map Charged Surfaces

Michael Skaug 1 Daniel Schwartz 1

1University of Colorado Boulder Boulder USA

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9:00 AM - J9.04
The Link between the Polarization/Relaxation Dynamics and Resistive Switching in Ca-doped BiFeO3 as Studied via Electrical Transport and SPM Techniques

Evgheni Strelcov 1 Stephen Jesse 1 Chih- Hung Wang 2 Yung-Chun Teng 2 Ying Hao Chu 2 Ivan I. Kravchenko 1 Sergei V. Kalinin 1

1Oak Ridge National Laboratory Oak Ridge USA2National Chiao Tung University Hsinchu Taiwan

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9:00 AM - J9.05
Effects of Electron Irradiation during High Temperature In-situ TEM Observations of Pb Nanoparticles in Silica

Flavia Piegas Luce 1 Erwan Oliviero 2 Daniel L. Baptista 1 Gustavo de M. Azevedo 1 Fernando C. Zawislak 1 Paulo F. P. Fichtner 1 3 4

1Universidade Federal do Rio Grande do Sul Porto Alegre Brazil2CNRS-IN2P3-Universitamp;#233; Paris-Sud Orsay France3Universidade Federal do Rio Grande do Sul Porto Alegre Brazil4Universidade Federal do Rio Grande do Sul Porto Alegre Brazil

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9:00 AM - J9.08
First Principles NEXAFS Simulations of N-donor Uranyl Complexes

Das Pemmaraju 1 Ran Duan 5 Roy Copping 2 B. Jeon 4 3 Andrew Canning 3 David K Shuh 2 David Prendergast 1

1Lawrence Berkeley National Lab Berkeley USA2Lawrence Berkeley National Lab Berkeley USA3Lawrence Berkeley National Lab Berkeley USA4University of California Davis USA5Peking University Beijing China

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9:00 AM - J9.09
Effect of Transition-metal Additives on Dehydrogenation Kinetics of MgH2

Anindya Roy 1 Anderson Janotti 1 Chris G. Van de Walle 1

1University of California Santa Barbara Santa Barbara USA

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9:00 AM - J9.10
Structural Changes in Porous Polyolefin Separator Materials Due to Mechanical Strain Characterized by Ex Situ and In Situ Xrd

Kevin J Rhodes 1 Sandeep Rekhi 2 Jennifer Zhu 3 Anandan Venkataramani 1 Andrews Drews 1

1Ford Motor Company Dearborn USA2PANalytical Inc. Westborough USA3California Institute of Technology Pasadena, USA

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9:00 AM - J9.11
Transition Metal K-edge XANES for Li-rich Layered Cathode Material: First-principles Study

Tomoyuki Tamura 1 Ryo Kobayashi 1 Shuji Ogata 1 Tsukuru Ohwaki 2 Atsushi Ito 2

1Nagoya Institute of Technology Nagoya-shi Japan2Nissan Motor Co., Ltd. Yokosuka Japan

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9:00 AM - J9.12
In-situ Characterization of Radiation Damage in 3C-SiC Using Electrical Measurements

Matthew Cabral 1 Christopher Hardiman 1 Steven Shannon 1 William Weber 2 3 Yanwen Zhang 2 3

1North Carolina State University Raleigh USA2University of Tennessee Knoxville USA3Oak Ridge National Laboratory Oak Ridge USA

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9:00 AM - J9.14
In-situ Raman Spectroscopy and X-Ray Diffraction Studies of the Structural Transformations Leading to the SrCu2O2 Phase from Strontium-copper Oxide Thin Films Deposited by MOCVD

Afzal Khan 1 2 Odette Chaix-Pluchery 2 Herve Roussel 2 Carmen Jimenez 2 Jean-Luc Deschanvres 2

1University of Peshawar, Pakistan Peshawar Pakistan2Grenoble INP Grenoble France

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9:00 AM - J9.17
Probing the Thermal Collapse of PNIPAM Grafts by Quantitative In Situ Ellipsometry

Stefan Kooij 1 Xiaofeng Sui 2 Mark Hempenius 2 Harold Zandvliet 1 Julius Vancso 2

1MESA+ Institute for Nanotechnology, University of Twente Enschede Netherlands2MESA+ Institute for Nanotechnology, University of Twente Enschede Netherlands

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J5: XRAY I (Diffraction)
Session Chairs
Eric Stach
Gyula Eres
Wednesday AM, April 03, 2013
Moscone West, Level 2, Room 2008

9:15 AM - *J5.01
Watching Energy Storage Materials in Operation: In-Situ X-Ray Diffraction and Microscopy

Michael Toney 1

1SLAC National Accelerator Laboratory Menlo Park USA

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