2019 MRS Spring Meeting & Exhibit

Symposium CP03: Advances in in situ Techniques for Diagnostics and Synthetic Design of Energy Materials

2019-04-23   Show All Abstracts

Symposium Organizers

Chengjun Sun, Argonne National Laboratory
Jenny Lockard, Rutgers, The State University of New Jersey
Feng Wang, Brookhaven National Laboratory
Markus Winterer, University of Duisburg-Essen
CP03.01: Fast Transmission Electron Microscopy
Session Chairs
Jennifer Dionne
Chengjun Sun
Tuesday AM, April 23, 2019
PCC West, 100 Level, Room 101 C

10:30 AM - CP03.01.01
Development of a Dynamic Environment Transmission Electron Microscope for the Study of Ultrafast Light-Induced Phenomena in Nanoscale Materials

Renske van der Veen1

University of Illinois at Urbana-Champaign1

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11:00 AM - CP03.01.02
An Open Cell System for Probing Nanoparticles Under Illumination in Aqueous Solutions in an Environmental Transmission Electron Microscope

Barnaby Levin1,Diane Haiber1,Qianlang Liu1,2,Peter Crozier1

Arizona State University1,Intel Corporation2

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11:15 AM - CP03.01.03
Composition Analysis by EDS at Elevated Temperatures in STEM and SEM

Meiken Falke1,Igor Nemeth1

Bruker Nano GmbH1

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11:30 AM - CP03.01.04
In Situ Atomic-Scale Observation of Intermediate Pathways of Melting and Crystallization of Supported Bi-Nanoparticles in the TEM

Leonard Francis1

International Iberian Nanotechnology Laboratory1

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11:45 AM - CP03.01.05
Effects of Pulsed Electron-Beam Characteristics on Radiation-Sensitive Materials for Energy Applications

Elisah VandenBussche1,David Flannigan1

University of Minnesota1

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CP03.02: X-Ray Photoelectron and Electron Energy-Loss Spectroscopy
Session Chairs
Robert Schlögl
Markus Winterer
Tuesday PM, April 23, 2019
PCC West, 100 Level, Room 101 C

1:30 PM - CP03.02.01
Investigation of Aqueous Interfaces Using Ambient Pressure XPS

Hendrik Bluhm1,2

Lawrence Berkeley National Laboratory1,Fritz Haber Institute of the MPG2

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2:00 PM - CP03.02.02
Observing Reactions at Surfaces with Fast and Dynamic XPS

Christian Kaiser1,Burkhard Krömker1,Georg Prümper1

Sigma Surface Science GmbH1

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2:15 PM - CP03.02.03
The Role of First Principles Calculations in Interpreting Core Level X-Ray Photoelectron Spectra of Complex Heterogeneous Systems

Juhan Matthias Kahk1,Johannes Lischner1

Imperial College London1

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2:30 PM - CP03.02.04
Electron Energy-Loss Spectroscopy for Designing Plasmonic Catalysts

Renu Sharma1,2,Wei-Chang Yang1,2,Alina Bruma1,2,Canhui Wang1,2

National Institute of Standards and Technology1,University of Maryland2

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3:00 PM -
BREAK


CP03.03: In Situ/In Operando Observation of Catalysis and Catalysts
Session Chairs
Zhenxing Feng
Jenny Lockard
Tuesday PM, April 23, 2019
PCC West, 100 Level, Room 101 C

3:30 PM - CP03.03.01
Operando Spectro-Microscopy for Electro-Catalysts

Robert Schlögl1,2

MPI for Chemical Energy Conversion1,Frtiz Haber Institute of the Max Planck Society2

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4:00 PM - CP03.03.02
Elucidating the Effects of Chemical Potential and Ligands on Nonequilibrium Etching of Nanocrystals Using Graphene Liquid Cell TEM

Matthew Hauwiller1,Justin Ondry1,Paul Alivisatos1

University of California, Berkeley1

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4:15 PM - CP03.03.03
In Situ Diagnostics of 2D Materials Synthesis and Heterogeneity—Closing the Loop for Functional Optoelectronic Materials

David Geohegan1,Yu-Chuan Lin1,Yiling Yu1,Chenze Liu2,Gerd Duscher2,Alex Strasser1,3,Alexander Puretzky1,Kai Wang1,Mina Yoon1,Christopher Rouleau1,Stela Canulescu4,Philip Rack2,Liangbo Liang1,Gyula Eres1,Kai Xiao1

Oak Ridge National Laboratory1,University of Tennessee2,Texas A&M University3,Technical University of Denmark4

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4:30 PM - CP03.03.04
About Using In Situ and Operando Characterization to Characterize Catalysts

Jeroen van Bokhoven1

ETH Zurich-PSI1

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CP03.04: Poster Session: Advances in In Situ Techniques for Diagnostics and Synthetic Design of Energy Materials
Session Chairs
Jenny Lockard
Chengjun Sun
Markus Winterer
Markus Winterer
Tuesday PM, April 23, 2019
PCC North, 300 Level, Exhibit Hall C-E

5:00 PM - CP03.04.01
Light-Driven Liquid Cell Transmission Electron Microscopy to Study Photocatalytic Materials

Khim Karki2,Noah Glachman1,Noah Geller1,Alexander Shea1,Daan Hein Alsem2,Deep Jariwala1,Eric Stach1

University of Pennsylvania1,Hummingbird Scientific2

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5:00 PM - CP03.04.02
Revealing Non-Thermal Equilibrium Dynamics of Metal Films by In Situ Heating and Ultrafast Transmission Electron Microscopy

Zhiwei Wang1,Deshuai Li1,Zhong Lin Wang1

Chinese Academy of Sciences1

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5:00 PM - CP03.04.03
Probing Semiconductor Photocatalyst Surface Intermediates and Band Edge Energies via Ambient Pressure XPS on CO2 Photoreduction

Hsiang-Ting Lien1,Yi-Fan Huang2,Yu-Chung Chang1,Yaw-Wen Yang3,Kuei-Hsien Chen2,1,Li-Chyong Chen1

National Taiwan University1,Academia Sinica2,National Synchrotron Radiation Research Center3

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5:00 PM - CP03.04.04
In Situ Analysis and Simulation of Heat Generation During Charging and Discharging of Ni-Rich Layered Oxide Cathode

Gahee Kim1

SAIT1

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5:00 PM - CP03.04.05
Compositional and Structural Evolution of Ultra-Thin Nickel Silicide Films as Studied by In Situ Low- and Medium-Energy-Ion-Scattering

Tuan Tran1,Lukas Jablonka1,Zhen Zhang1,Daniel Primetzhofer1

Uppsala University1

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5:00 PM - CP03.04.06
Rapid High Shear Viscosity Measurements Using a Microfluidic Rheometer

Matt Vanden Eynden1,Thanina Amiar2,Hubert Ranchon2,Gerard Meunier2

Formulaction, Inc.1,Formulaction2

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5:00 PM - CP03.04.07
Dopant Profiling Using Low-Voltage SEM for GaN Power Electronics

Shanthan Reddy Alugubelli1,Houqiang Fu1,Kai Fu1,Hanxiao Liu1,Yuji Zhao1,Fernando Ponce1

Arizona State University1

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5:00 PM - CP03.04.08
Non-Uniform Mg Doping in GaN Epilayers on Mesa Structures

Hanxiao Liu1,Houqiang Fu1,Kai Fu1,Shanthan Reddy Alugubelli1,Yuji Zhao1,Fernando Ponce1

Arizona State University1

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5:00 PM - CP03.04.09
Identification of Point Defects in BAlN Using High-Resolution Electron Energy Loss Spectroscopy

Shuo Wang1,Katia March1,Peter Rez1,Fernando Ponce1

Arizona State University1

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5:00 PM - CP03.04.10
Adapting the e-Beam of an SEM as a Quantitative Nanoscale Heat Source

Pengyu Yuan1,2,3

University of California, Merced1,University of California, Berkeley2,Lawrence Berkeley National Laboratory3

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5:00 PM - CP03.04.11
In Situ Electron Beam Induced Current STEM Measurements of the Minority Carrier Diffusion Length in n-GaN

Zoey Warecki1,Andrew Armstrong2,Alec Talin2,John Cumings1

University of Maryland1,Sandia National Laboratories2

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5:00 PM - CP03.04.12
In Situ Study of the Thermally Activated Self-Assembly of Carboxylated Polythiophene for Photovoltaic Applications

Teddy Salim1,Pio John Buenconsejo1,Yeng Ming Lam1

Nanyang Technological University1

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5:00 PM - CP03.04.13
In Situ TEM Biasing Experiments with Easy-to-Move Mobile Probes

Julio Rodriguez Manzo1,Khim Karki1,Daan Hein Alsem1,Norman Salmon1

Hummingbird Scientific1

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5:00 PM - CP03.04.14
Exploring the Interfacial Structure in Aqueous Colloidal Tin Dioxide Dispersions

Viktor Mackert1,Thomas Winter1,Markus Winterer1

Universität Duisburg-Essen1

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5:00 PM - CP03.04.15
Designing Perovskite Nanoparticles to Probe Structural Changes During Catalytic Activity by In Situ X-Ray Absorption Spectroscopy

Jeremias Geiss1,Markus Winterer1

University of Duibsurg-Essen1

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5:00 PM - CP03.04.16
Coupling Operando Electrochemical Mass Spectrometry with Post-Mortem Analysis of Electrodes for Revealing the Degradation Mechanisms of Electrochemical Capacitors During High Voltage Operation

Francois Beguin1,Patryk Przygocki1,Paula Ratajczak1

Poznan University of Technology1

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5:00 PM - CP03.04.17
Colossal Transformations in Metal-Organic Frameworks with Ultrahigh Porosity

Stefan Kaskel1,2

Fraunhofer IWS1,TU Dresden2

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5:00 PM - CP03.04.18
Fundamental Understanding of the Effects of Molten Salts on MgO for the Intermediate−CO2 Adsorption via In Situ DRIFTS Techniques

Wanlin Gao1,Qiang Wang1

Beijing Forestry University1

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5:00 PM - CP03.04.19
In Situ Measurements of Plasma-Surface Interactions via Time Domain Thermoreflectance—Electron Heating, Surface Cooling and Chemical Reactions in Materials

Patrick Hopkins1,John Tomko1,Scott Walton2

University of Virginia1,U.S. Naval Research Laboratory2

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5:00 PM - CP03.04.20
Molecular Beam Epitaxy Grown Core-Shell Gallium Arsenide Nanowire Solar Cells on Silicon Substrate

M. Hadi Tavakoli Dastjerdi1,Ray LaPierre2

Massachusetts Institute of Technology1,McMaster University2

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5:00 PM - CP03.04.21
Characterization of Single Solar Cell Nanowires Using a Scanning Tunneling Microscope–Scanning Electron Microscope Setup

Jonatan Holmér1,Lunjie Zeng1,Thomas Nordqvist2,Peter Krogstrup2,Jesper Nygård2,Ludvig de Knoop1,Eva Olsson1

Chalmers University of Technology1,University of Copenhagen2

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5:00 PM - CP03.04.22
In Situ Transient Absorption Spectroscopy During Materials Formation

Cathy Wong1

University of Oregon1

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5:00 PM - CP03.04.23
In Situ Studies of Ion Transport in Electrolyte and Electrolyte/Lithium Interfacial Reactions

Yuan Yang1

Columbia University1

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5:00 PM - CP03.04.24
The Visualization of Single Grain Evolution in Operando Cathode Materials with the Coherent Hard X-Ray Diffraction

Luxi Li1,Ross Harder1,Yingying Xie2,Evan Maxey1

Argonne National Laboratory1,Shanghai Jiao Tong University2

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5:00 PM - CP03.04.25
Tracking the Underlying Redox Mechanism in Na2FeP2O7 Pyrophosphate Cathode for Sodium-Ion Batteries

Ritambhara Gond1,Prabeer Barpanda1

Indian Institute of Science1

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5:00 PM - CP03.04.26
In Situ and Operando Soft X-Ray Spectroscopy of Energy-Relevant Materials

Lothar Weinhardt1,2,Dirk Hauschild1,Monika Blum3,2,Clemens Heske1,2

Karlsruhe Institute of Technology (KIT)1,University of Nevada, Las Vegas2,Lawrence Berkeley National Laboratory3

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5:00 PM - CP03.04.27
Systematic Design of High Performance Lithium-Sulfur Battery Using Efficient Polysulfide Adsorbent Porous Host Materials

Tilahun Zegeye1

National Taiwan University of Science and Technology1

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2019-04-24   Show All Abstracts

Symposium Organizers

Chengjun Sun, Argonne National Laboratory
Jenny Lockard, Rutgers, The State University of New Jersey
Feng Wang, Brookhaven National Laboratory
Markus Winterer, University of Duisburg-Essen
CP03.05: X-Ray Diffraction and Batteries
Session Chairs
Ashfia Huq
Feng Wang
Wednesday AM, April 24, 2019
PCC West, 100 Level, Room 101 C

8:30 AM - CP03.05.01
In Situ Synchrotron X-Rays Studies on the Synthesis of Energy Materials for Li-Ion Battery

Jianming Bai1

Brookhaven National Laboratory1

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9:00 AM - CP03.05.02
Large Area and Multimodal Study of Li-Ion Batteries with New In Situ Technologies

Stefanie Freitag1

Zeiss1

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9:15 AM - CP03.05.03
In Situ Probing of Anionic Redox in Li-Rich Layered Cathodes

Chong Yin1,2,Bao Qiu2,Jianming Bai3,Zhaoping Liu2,Feng Wang1

Brookhaven National Laboratory1,Ningbo Institute of Materials Technology and Engineering, Chinese Academy of Sciences2,Brookhaven Nation Laboratory3

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9:30 AM - CP03.05.04
Bismuth as Rechargeable Lithium-Ion Battery Anode—A Fundamental Study Using In Situ Synchrotron XRD and In Situ TEM

Yifei Yuan1,Wentao Yao1,Vitaliy Yurkiv1,Farzad Mashayek1,Jun Lu2,Khalil Amine2,Reza Shahbazian-Yassar1

University of Illinois at Chicago1,Argonne National Laboratory2

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9:45 AM - CP03.05.05
Cationic Ordering Coupled to Reconstruction of Basic Building Units During Synthesis of High-Ni Layered Oxide Cathodes

Mingjian Zhang1,2,Gaofeng Teng2,Jianming Bai1,Feng Pan2,Feng Wang1

Brookhaven National Lab1,Peking University2

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10:00 AM -
BREAK


CP03.06: Neutron Scattering and Battery Related Materials
Session Chairs
Steve Heald
Feng Wang
Wednesday AM, April 24, 2019
PCC West, 100 Level, Room 101 C

10:30 AM - CP03.06.01
Following In Situ Synthesis Using Neutron Powder Diffraction

Ashfia Huq1

Oak Ridge National Laboratory1

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11:00 AM - CP03.06.02
Zooming in to Sub-Nanoscale—In Situ Studies of Porous Materials Using Recently Upgraded Neutron Spectrometer NEAT at Helmholtz Zentrum Berlin

Margarita Russina1,Gerrit Guenther1,Veronika Grzimek1

Helmholtz-Zentrum Berlin für Materialien und Energie1

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11:15 AM - CP03.06.03
In Situ Study of Thermal and Electrochemical Properties of LiCoO2 Thin Films by Raman Spectroscopy

Denis Rouchon1,Van Hoan Le2,Christophe Secouard1,Lucie Le Van-Jodin1

CEA/LETI1,CNRS2

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11:30 AM - CP03.06.04
Silicide-Nanowire Anchored on the Inner Surface of 3D Graphene Micro-Tubular as an Anode Material for Li-Ion Battery

Chang Won Jun1,Won Il Park1

Hanyang University1

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11:45 AM - CP03.06.05
Proving Structural Evolutions of Silicon Anode in an Advanced Li-Ion Batteries Using In Situ Synchrotron X-Ray Studies

Sungwon Lee1,Sungsik Lee1,Jaewook Lee2,Randall Winans1

Argonne National Laboratory1,LG Chem Ltd2

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CP03.07: X-Ray Spectroscopy and Battery Related Materials
Session Chairs
Anatoly Frenkel
Jenny Lockard
Wednesday PM, April 24, 2019
PCC West, 100 Level, Room 101 C

1:30 PM - CP03.07.01
X-Ray Spectroscopic Studies of Energy Storage Systems

Mahalingam Balasubramanian1,Jason Croy1

Argonne National Laboratory1

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2:00 PM - CP03.07.02
In Situ XAS Studies of Layered Double Hydroxide Catalysts for Electrochemical Oxygen Evolution Reaction

Maoyu Wang1,Zhenxing Feng1

Oregon State University1

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2:15 PM - CP03.07.03
Laboratory-Based Hard X-Ray Photoelectron Spectrometer for the Study of Advanced and Complex Materials

Anna Regoutz1,Manfred Mascheck2,Tomas Wiell2,Susanna Eriksson2,Cristopher Liljenberg2,Kornelius Tetzner1,Benjamin Williamson3,David Scanlon3,Paul Palmgren1

Imperial College London1,Scienta Omicron2,University College London3

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2:30 PM -
BREAK


CP03.08: X-Ray Spectroscopy and Catalysis
Session Chairs
Mahalingam Balasubramanian
Markus Winterer
Wednesday PM, April 24, 2019
PCC West, 100 Level, Room 101 C

3:30 PM - CP03.08.01
In Situ Determination of Active Species and Active Sites in Water Gas Shift Reaction Over Pt/CeO2 Catalysts

Anatoly Frenkel1,3,Yuanyuan Li1,Matthew Kottwitz2,Ralph Nuzzo2

Stony Brook University, The State University of New York1,University of Illinois at Urbana-Champaign2,Brookhaven National Laboratory3

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4:00 PM - CP03.08.02
Unveiling Site-Selective CO Disproportionation Mediated by Electron Beam Excited Localized Surface Plasmon Resonance

Wei-Chang Yang1,2,Canhui Wang1,2,Henri J. Lezec1,Renu Sharma1

National Institute of Standards and Technology1,University of Maryland2

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4:15 PM - CP03.08.03
X-Ray Absorption Study on Iron(III)Acetylacetonate Vapor and Nanoparticles Produced from It

Oleksandr Levish1,Markus Winterer1

Universität Duisburg-Essen1

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4:30 PM - CP03.08.04
In Situ X-Ray Absorption Spectroscopy Studies of Catalysts in Electrochemical Reactions

Zhenxing Feng1

Oregon State University1

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2019-04-25   Show All Abstracts

Symposium Organizers

Chengjun Sun, Argonne National Laboratory
Jenny Lockard, Rutgers, The State University of New Jersey
Feng Wang, Brookhaven National Laboratory
Markus Winterer, University of Duisburg-Essen
CP03.09: Small Angle Scattering, Ion Scattering and Related Methods
Session Chairs
Jianming Bai
Feng Wang
Thursday AM, April 25, 2019
PCC West, 100 Level, Room 101 C

8:30 AM - CP03.09.01
Exploring Pore Formation of Atomic Layer-Deposited Overlayers by In Situ Small Angle X-Ray Scattering

Tao Li1,2

Northern Illinois University1,Argonne National Laboratory2

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9:00 AM - CP03.09.02
In Situ Small-Angle X-Ray Scattering Observation of Electrophoretic Deposition at the Nanoscale

Viktor Mackert1,Markus Winterer1

Universität Duisburg-Essen1

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9:15 AM - CP03.09.03
Advanced Setups for In Situ Growth and Characterization of Materials by Ion Beams

Tuan Tran1,Barbara Bruckner1,Karim Kantre1,Marcos Moro1,Mauricio Sortica1,Silma Correa1,Svenja Lohmann1,Valentina Paneta1,Daniel Primetzhofer1,2

Uppsala University1,Tandem Laboratory2

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9:30 AM - CP03.09.04
Cluster Tool for In Situ Processing and Comprehensive Characterization of Energy Materials at High Temperatures

Matthias Krause1,Robert Wenisch1,Frank Lungwitz1,Irene Heras2,Daniel Janke1,Ibon Azkona3,Ramon Escobar Galindo4,Sibylle Gemming1,5

Helmholtz-Zentrum Dresden-Rossendorf1,University of Salamanca2,Metal Estalki S.L.3,Universidad de Cádiz4,Technische Universität Chemnitz5

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9:45 AM - CP03.09.05
Probing Prospective Electrode Materials for Next Generation High-Energy Density Batteries by Advanced Focused Electron Beam and Ion Beam Techniques

Vladimir Oleshko1,Saya Takeuchi1,2,Alison Kriz3,William McGehee1,Andrei Kolmakov1,John Cumings3,Jabez McClelland1,Christopher Soles1

National Institute of Standards and Technology1,Theiss Research2,University of Maryland3

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10:00 AM -
BREAK


CP03.10: In Situ Scanning/Transmission Electron Microscopy
Session Chairs
Thursday AM, April 25, 2019
PCC West, 100 Level, Room 101 C

10:30 AM - CP03.10.01
The Light Years—Concurrent Optical and Transmission Electron Spectroscopy to Visualize Photo-Chemical Transformations with Nanometer-Scale Resolution

Jennifer Dionne1,Michal Vadai1,Fariah Hayee1,Katherine Sytwu1,Daviel Angell1,Amr Saleh1

Stanford University1

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11:00 AM - CP03.10.02
Boron Nitride Nanotube Electron-Beam Induced Oxidation at 80keV

Hsin-Yun Chao1,2,Dmitri Golberg3,Cheol Park4,Renu Sharma2,John Cumings1

University of Maryland1,National Institute of Standards and Technology2,Queensland University of Technology3,NASA Langley Research Center4

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11:15 AM - CP03.10.03
Advanced In Situ and Ex Situ S/TEM Probing of Interfacial Process in Rechargeable Batteries

Chongmin Wang1

Pacific Northwest National Laboratory1

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11:30 AM - CP03.10.04
Cu2O Island Growth Process During Cu(100) Oxidation Revealed by Correlated In Situ Environmental TEM and Multiscale Simulations

Meng Li1,Matthew Curnan1,Wissam Saidi1,Judith Yang1

University of Pittsburgh1

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11:45 AM - CP03.10.05
Real-Time Imaging of Reducible Oxide Nanoparticle Surface Reconstructions Using Time-Resolved Aberration-Corrected Transmission Electron Microscopy

Ethan Lawrence1,Barnaby Levin1,Benjamin Miller2,Peter Crozier1

Arizona State University1,Gatan, Inc.2

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