Meetings & Events

 

2013 MRS Fall Meeting Logo2013 MRS Fall Meeting & Exhibit

December 1-6, 2013 | Boston
Meeting Chairs: Charles Black, Elisabetta Comini, Gitti Frey, Kristi Kiick, Loucas Tsakalakos

Symposium FF : Characterization of Energy Materials In-Situ and Operando

2013-12-02   Show All Abstracts

Symposium Organizers

Ilke Arslan, Pacific Northwest National Laboratory
Eric Stach, Brookhaven National Laboratory
Yury Gogotsi, Drexel University
Liqiang Mai, Wuhan University of Technology

Symposium Support

FEI Co
Fischione Instruments, Inc.
Wuhan University of Technology
FF2: In-situ and Operando Methods in Energy Storage I
Session Chairs
Ilke Arslan
Monday PM, December 02, 2013
Hynes, Level 3, Room 310

2:30 AM - FF2.01
The Effect of Bi Additives on Zn Morphology Imaged in situ Using Liquid Cell Transmission Electron Microscopy

Jeung Hun Park 1 2 Mark C. Reuter 2 Nicholas M. Schneider 3 Haim H. Bau 3 Daniel A. Steingart 4 Suneel Kodambaka 1 Frances M. Ross 2

1University of California Los Angeles Los Angeles USA2IBM T. J. Watson Research Center Yorktown Heights USA3University of Pennsylvania Philadelphia USA4Princeton University Princeton USA

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2:45 AM - FF2.02
Transmission Electron Microscopy in Ionic Liquids - Particle Motion Visualization

Ulrich Mansfeld 1 Stephanie Hoeppener 1 2 Ulrich S. Schubert 1 2

1Friedrich Schiller University Jena Jena Germany2Jena Center of Soft Matter (JCSM) Jena Germany

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3:00 AM - *FF2.03
In-Situ TEM Study of Electrochemical Cell: In Terms of Battery, What We Have Learned and Where We Should be Heading

Chongmin Wang 1 Meng Gu 1 Lucas R Parent 1 Patricia Abellan Baeza 1 Xu Wu 1 Suntharampillai Thevuthasan 1 Donald R Baer 1 Ji-Guang Zhang 1 Jun Liu 1 Ilke Arslan 1 Raymond R Unocic 2 Nigel D Browning 1

1Pacific Northwest National Lab Richland USA2Oak Ridge National Laboratory Oak Ridge USA

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3:30 AM - FF2.04
Visualizing In Situ Electrochemical Deposition and Dendrite Growth with the Nanoaquarium

Nicholas M Schneider 1 Jeung Hun Park 2 3 Joseph M Grogan 1 Suneel Kodambaka 2 Daniel A Steingart 4 Frances M Ross 3 Haim H Bau 1

1University of Pennsylvania Philadelphia USA2University of California - Los Angeles Los Angeles USA3IBM T. J. Watson Research Center Yorktown Heights USA4Princeton University Princeton USA

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3:45 AM - FF2.05
Revealing Materials Transformation during Electrochemical Processes in Liquid Electrolytes

Zhiyuan Zeng 1 Kaiyang Niu 1 Wen-I Liang 1 Haimei Zheng 1

1Lawrence Berkeley National Lab Berkeley USA

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4:00 AM -
BREAK

4:30 AM - FF2.06
In-situ TEM Observation on Multiple-Stripe Lithiation Process in Individual SnO2 Nanowires

Scott X. Mao 1 Li Zhong 1 Jianyu Huang 2

1University of Pittsburgh Pittsburgh USA28915 Hampton Ave NE Albuquerque USA

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4:45 AM - FF2.07
High-Temperature In Situ Observation of Crystal Evaporation in LiFePO4 at Atomic Resolution

Sung-Yoon Chung 1 2

1KAIST Daejeon Republic of Korea2Nalphates Wilmington USA

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5:00 AM - FF2.08
In-situ TEM Observation of Electrochemistry in All-Solid-State Nano-Batteries

Ziying Wang 1 Dhamodaran Santhanagopalan 1 Danna Qian 1 Feng Wang 2 Jason Graetz 2 Juchuan Li 3 Nancy Dudney 3 Shirley Meng 1

1University of California San Diego La Jolla USA2Brookhaven National Lab Upton USA3Oak Ridge National Lab Oak Ridge USA

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5:15 AM - FF2.09
In-situ Characterization of Single Nanowire Electrochemical Devices

Liqiang Mai 1

1Wuhan University of Technology Wuhan China

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5:30 AM - FF2.10
Fast Electrogravimetric Methods for Investigating Electrode Materials in Electrochemical Conversion Devices: Application to Electrodeposited MnO2 Thin Films

Claude Gabrielli 1 Alain Pailleret 1 Hubert Perrot 1 Carlota Ridruejo 1 Ozlem Sel 1

1LISE, UPMC Paris 6, CNRS Paris France

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5:45 AM - FF2.11
Pseudocapacitive Phenomena at the Electrode/Electrolyte Interface Investigated by In-Situ Electrochemical Techniques

Mikolaj Meller 1 Krzysztof Fic 1 Grzegorz Lota 1 Elzbieta Frackowiak 1

1Poznan University of Technology Poznan Poland

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FF3: Poster Session: In-situ and Operand Methods in Catalysis and Energy Storage
Session Chairs
Eric Stach
Monday PM, December 02, 2013
Hynes, Level 1, Hall B

9:00 AM - FF3.01
In situ TEM Study of Hydrogenation of Mg Films Decorated with Pd Manoparticles

Sang Chul Lee 1 Chia-Jung Chung 1 Ai Leen Koh 2 Bruce Clemens 1 Robert Sinclair 1 2

1Stanford University Stanford USA2Stanford University Stanford USA

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9:00 AM - FF3.02
Dynamics of Redox Behavior in SrCoOx Epitaxial Films

Dillon Fong 1 Hubert Renevier 2 Valentina Cantelli 2 Marie-Ingrid Richard 3 4 Chad Folkman 1 Hyoungjeen Jeen 5 Ho Nyung Lee 5

1Argonne National Laboratory Argonne USA2Grenoble INP Grenoble France3Aix-Marseille Universitamp;#233; Marseille France4European Synchrotron Radiation Facility Grenoble France5Oak Ridge National Laboratory Oak Ridge USA

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9:00 AM - FF3.03
High Temperature Environmental Scanning Electron Microscopy of Ni/YSZ Surfaces after Exposure to PH3

Mahfuzur Jony 1 Harry Finklea 1 Mingjia Zhi 2

1West Virginia University Morgantown USA2West Virginia University Morgantown USA

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9:00 AM - FF3.04
In-situ Characterization of Catalytic Reactions Using Environmental Cell TEM

Daan Hein Alsem 1 Robert Colby 2 See Wee Chee 1 Bernd Kabius 2 Norman Salmon 1

1Hummingbird Scientific Lacey USA2Pacific Northwest National Laboratory Richland USA

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9:00 AM - FF3.05
Atmospheric Pressure Electron Beam Induced Current Microscopy on Working Individual Metal Oxide Nanowire Gas Sensor

Jie Zhang 1 Yangmingyue Liu 1 Andrei Kolmakov 1 2

1SIUC/NIST Carbondale USA2NIST Gaithersburg USA

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9:00 AM - FF3.08
Nanoscale Photovoltaic Performance in Micropatterned CdTe-CdS

Yasemin Kutes 1 James L. Bosse 1 Jose Luis Cruz-Campa 2 Erik D. Spoerke 2 David Zubia 3 Brandon Aguirre 3 Bryan D. Huey 1

1University of Connecticut Storrs USA2Sandia National Laboratories Albuquerque USA3University of Texas at El Paso El Paso USA

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9:00 AM - FF3.09
Electrochemically Tunable Thermal Conductivity of Lithium Cobalt Oxide

Jiung Cho 1 Mark D Losego 2 Hui Gang Zhang 1 Honggyu Kim 1 Jianmin Zuo 1 Ivan Petrov 1 David G. Cahill 1 Paul V. Braun 1

1University of Illinois at Urbana-Champaign Urbana USA2North Carolina State University Raleigh USA

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9:00 AM - FF3.10
In situ Investigation of Stress Evolution and Failure Mechanisms in High Voltage Ta Oxide Capacitors

Xin Su 1 Mark Viste 2 Joachim Hossick-Schott 2 Brian W. Sheldon 1

1Brown University Providence USA2Medtronic Minneapolis USA

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9:00 AM - FF3.12
Neutron Reflectometry: A Unique Probe for the In Situ Study of Interfacial Reactions on Thin Film Electrical Energy Storage Materials

Jim Browning 1 Gabriel M Veith 1 Wyatt Tenhaeff 1 Loic Baggetto 1 Nancy J Dudney 1 Jong Keum 1

1Oak Ridge National Laboratory Oak Ridge USA

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9:00 AM - FF3.13
In-Situ Monitoring of Reversible Thermal Transport in Lithium Ion Battery

Yongjie Hu 1 Gang Chen 1

1Massachusetts Institute of Technology Cambridge USA

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9:00 AM - FF3.14
Combining In-situ Mechanical, Ellipsometric and Spectrometric Tools during Growth of 3D Porous Anodic Silica

Frederic Blaffart 1 Ronny Santoro 1 Hosni Idrissi 1 2 Joris Proost 1

1Universitamp;#233; catholique de Louvain Louvain-la-Neuve Belgium2University of Antwerp Antwerp Belgium

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9:00 AM - FF3.15
In-situ Lithiation Behavior of Diverse Si Nanostructures for Li Ion Battery

In-Suk Choi 1

1Korea Institute of Science and Technology Seoul Republic of Korea

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9:00 AM - FF3.16
In-situ High-Resolution TEM Study of Lithiation Mechanisms in Si and Ge Electrodes

Yang Liu 1 Xiaohua Liu 1 Katherine L Jungjohann 1 Shadi A Dayeh 2 3 Sulin Zhang 4 Ju Li 5 Ting Zhu 6

1Center for Integrated Nanotechnology (CINT), Sandia National Laboratories Albuquerque USA2Los Alamos National Laboratory Los Alamos USA3University of California, San Diego La Jolla USA4Pennsylvania State University University Park USA5Massachusetts Institute of Technology Cambridge USA6Georgia Institute of Technology Atlanta USA

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9:00 AM - FF3.18
In-Situ Investigation of Oxidation Behavior of Ti3C2 for Energy Storage Applications

Hessam Ghassemi 1 Wayne Harlow 1 Olha Mashtalir 1 Maria Lukatskaya 1 Majid Beidaghi 1 Yury Gogotsi 1 Mitra Taheri 1

1Drexel Univ Philadelphia USA

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9:00 AM - FF3.20
High Throughput, In Situ Studies of Geometric Features in Patterned Electrodes

Robert Usiskin 1 Shingo Maruyama 3 Chris Kucharzyck 1 Ichiro Takeuchi 3 Sossina Haile 1 2

1Califorina Institute of Technology Pasadena USA2Califorina Institute of Technology Pasadena USA3University of Maryland College Park USA

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9:00 AM - FF3.21
In situ Chemomechanics of PrxCe1-xO2-delta; via Environmentally Controlled Nanoindentation

Jessica G Swallow 1 Jae Jin Kim 1 Sean R Bishop 1 2 Harry L Tuller 1 Krystyn J Van Vliet 1 3

1Massachusetts Institute of Technology Cambridge USA2Kyushu University Nishi-Ku Fukuoka Japan3Massachusetts Institute of Technology Cambridge USA

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9:00 AM - FF3.22
Ionic Liquid Electrolyte Dynamics in Porous Architectures of Supercapacitor Electrodes Determined via In situ Infrared Spectroelectrochemistry

Boris Dyatkin 1 Francis Richey 2 Yossef Elabd 2 Yury Gogotsi 1

1Drexel University Philadelphia USA2Drexel University Philadelphia USA

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9:00 AM - FF3.24
In-situ Spectroscopy of Spontaneous Dehydrogenation Reactions

Elsa Callini 1 Andreas Borgschulte 1 Andreas Zuettel 1

1Empa, Swiss Federal Laboratories Duebendorf Switzerland

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9:00 AM - FF3.25
Correlative Electron Microscopy and Photon Science Characterization of Working Catalysts

Eric Andrew Stach 1 Yuanyuan Li 2 Philipp Baumann 3 Dmitri Zakharov 1 Anatoly Frenkel 2

1Brookhaven National Laboratory Upton USA2Yeshiva University New York USA3University of Applied Sciences of Northeastern Switzerland Muttenz Switzerland

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9:00 AM -
FF3.19 TRANSFERRED TO FF2.02

9:00 AM -
FF3.11 Transferred to FF4.06

9:00 AM -
FF3.06 Transferred to FF1.04

FF1: In-situ and Operando Methods in Catalysis
Session Chairs
Ilke Arslan
Monday AM, December 02, 2013
Hynes, Level 3, Room 310

9:30 AM - FF1.01
Structural Tunability of Catalytic Properties of Pt-Alloy Nanoparticles: An In-situ Study of the Structure Evolution upon Oxidative/reductive Treatments

Shiyao Shan 1 Lefu Yang 1 Jin Luo 1 Valeri Petkov 2 Chuan-Jian Zhong 1

1State University of New York at Binghamton Binghamton USA2Central Michigan University Mt Pleasant USA

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9:45 AM - FF1.02
Active Sites of Gold-Ceria Catalysts for Water-Gas Shift Reaction: In-Situ Combined XAFS/DRIFTS under Transient Conditions

Rui Si 1 Yu Guo 2 Chun-Jiang Jia 2

1Shanghai Institute of Applied Physics, Chinese Academy Sciences Shanghai China2Shandong University Jinan China

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10:00 AM - *FF1.03
Synchrotrons, Catalysts and UOP: From Imaging to In situ Spectroscopy

Simon R Bare 1

1UOP LLC Des Plaines USA

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10:30 AM - FF1.04
2D Electron Transparent Membranes and Samples Platform for Ambient Pressure Photoelectron Imaging and Spectroscopy

Alexander Yulaev 1 Andrei Kolmakov 2

1SIUC/NIST Carbondale USA2NIST Gaithersburg USA

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10:45 AM - FF1.05
Size and Composition Selected Subnanometer Silver Catalysts for One Step Propylene Epoxidation: Understanding Function through In situ Studies

Eric Christopher Tyo 1 Bing Yang 1 Janae De Bartolo 2 Soenke Seifert 2 Randall E. Winans 2 Jeremy Kropf 3 John Katsoudas 5 Carlo Segre 5 Stefan Vajda 1 4 6

1Argonne National Laboratory Lemont USA2Argonne National Laboratory Lemont USA3Argonne National Laboratory Lemont USA4Argonne National Laboratory Lemont USA5Illinois Institute of Technology Chicago USA6Yale University New Haven USA

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11:00 AM -
BREAK

11:30 AM - *FF1.06
Atomic Level In Situ Probing of Materials Structure and Function for Energy Conversion Processes

Peter A Crozier 1

1Arizona State University Tempe USA

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12:00 PM - *FF1.07
Imaging Catalysts in the Working State

Stig Helveg 1

1Haldor Topsoe A/S Kgs. Lyngby Denmark

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12:30 PM - FF1.08
Study of Grain Growth and Defect Formation in Ag Thin Films by Planar TEM with In-situ Heating

Sophie Brossard 1 Florent Martin 1 Julie Bourgon 2

1Saint Gobain Recherche Aubervilliers France2ICMPE - CNRS Thiais France

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12:45 PM - FF1.09
In-situ TEM Study of Stability of Pd Nanoparticles in the Presence of Reactive Gases

Libor Kovarik 1 Arda Genc 2 Ayman Karim 1 Janos Szanyi 1 Ja-Hun Kwak 1 3 Charles Peden 1

1Pacific Northwest National Lab Richland USA2FEI Company Hillsboro USA3UNIST Ulsan Republic of Korea

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2013-12-03   Show All Abstracts

Symposium Organizers

Ilke Arslan, Pacific Northwest National Laboratory
Eric Stach, Brookhaven National Laboratory
Yury Gogotsi, Drexel University
Liqiang Mai, Wuhan University of Technology

Symposium Support

FEI Co
Fischione Instruments, Inc.
Wuhan University of Technology
FF5: In-situ and Operando Methods in Energy Storage III
Session Chairs
Eric Stach
Tuesday PM, December 03, 2013
Hynes, Level 3, Room 310

2:30 AM - FF5.01
In situ Total-Reflection Fluorescence X-Ray Absorption Spectroscopic Study on Electronic Structure at Cathode/Electrolyte Interface during Charge/Discharge Process

Yoshiharu Uchimoto 1 Yuki Orikasa 1

1Kyoto University Kyoto Japan

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2:45 AM - FF5.02
Kinetic Aspects of Electrochemical Reactions in Li2MnO3 Cathode Material for Rechargeable Li-Ion Batteries

Jatinkumar Rana 1 Marian Stan 2 Gerhard Schumacher 1 Ivo Zizak 1 John Banhart 1 3 Martin Winter 2

1Helmholtz-Zentrum Berlin famp;#252;r Materialien und Energie Berlin Germany2Institute of Physical Chemistry, MEET Battery Research Centre, University of Muenster Muenster Germany3Technische Universitamp;#228;t Berlin Berlin Germany

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3:00 AM - *FF5.03
Following Function in Real Time: New NMR and MRI Methods for Studying Structure and Dynamics in Batteries and Supercapacitors

Clare Grey 1 2

1University of Cambridge Cambridge United Kingdom2Stony Brook University Stony Brook USA

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3:30 AM - FF5.04
Enhanced Crystallisation of Li3.75Si in P-Doped Si-Nanowire Based Li-Ion Batteries: A Study by In Situ NMR

Ken Ogata 1 Stephan Hofmann 1 Clare Grey 2 3

1Cambridge University Cambridge United Kingdom2Cambridge University Cambridge United Kingdom3Stony Brook University New York United Kingdom

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3:45 AM - FF5.05
Real Time Magnetic Measurements in Lithium-Ion Batteries

Gregory Gershinsky 1 Laure Monconduit 2 David Zitoun 1

1Bar Ilan University Ramat Gan Israel2University Montpellier 2 Montpellier France

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4:00 AM -
BREAK

4:30 AM - FF5.06
Measuring Strain Evolution in Operando in Bicontinuous Silicon Inverse Opal Anodes for Lithium Ion Batteries Using X-Ray Diffraction

Matthew P. B. Glazer 1 Jiung Cho 2 Jonathan Almer 3 John Okasinski 3 Paul V. Braun 2 David C. Dunand 1

1Northwestern University Evanston USA2University of Illinois at Urbana-Champaign Urbana USA3Argonne National Laboratory Argonne USA

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4:45 AM - FF5.07
In-situ Study of Electrochemically-Driven Phase Transitions in LiMnyFe1-yPO4 Cathode Materials

Dorthe Ravnsbaek 1 Kai Xiang 1 Wenting Xing 1 Olaf Borkiewicz 2 Kamilla Wiaderek 2 Peter Chupas 2 Karena Chapman 2 Yet-Ming Chiang 1

1Massachusetts Institute of Technology Cambridge USA2Argonne National Laboratory Argonne USA

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5:00 AM - FF5.08
Ultrafast Chemical Charging of Lithium Iron Phosphate

Christian Kuss 1 David Lepage 1 Guoxian Liang 2 Steen Brian Schougaard 1

1Universitamp;#233; du Quamp;#233;bec amp;#224; Montramp;#233;al Montreal Canada2Clariant (Canada), Inc Candiac Canada

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5:15 AM - FF5.09
In-situ Atomic Force Microscopy (AFM) and Ultra-Small-Angle X-Ray Scattering (USAXS) for the Analysis of Zinc Electrodeposition from an Ionic Liquid Electrolyte

Jayme S. Keist 1 2 Christine A. Orme 2 Bassem S. El-Dasher 2 Sharon G. Torres 2 Jan Ilavsky 3 Frances M. Ross 4 Daniel A. Steingart 5 Paul K. Wright 1 James W. Evans 1

1University of California - Berkeley Berkeley USA2Lawrence Livermore National Laboratory Livermore USA3Argonne National Laboratory Argonne USA4IBM T. J. Watson Research Center Yorktown Heights USA5Princeton University Princeton USA

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5:30 AM - FF5.10
A New Electrochemical Cell for Rietveld Refinements of In-situ or Operando Neutron Powder Diffraction Data

Matteo Bianchini 1 2 3 Emmanuelle Suard 1 Christian Masquelier 2 Laurence Croguennec 3

1Institut Laue Langevin Grenoble France2Universitamp;#233; de Picardie Jules Verne Amiens France3Universitamp;#233; de Bordeaux Bordeaux France

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FF4: In-situ and Operando Methods in Energy Storage II
Session Chairs
Yury Gogotsi
Tuesday AM, December 03, 2013
Hynes, Level 3, Room 310

9:15 AM - *FF4.01
Complementary In Situ and In Operando Studies of Complex Energy Storage Systems Leveraging Low Cost, Abundant Materials

Daniel A Steingart 1 Joshua Gallaway 5 Mylad Chamoun 1 Benjamin Hertzberg 1 Frances Ross 3 Can Erdonmez 4 Diviraj Desai 5 Christine Orme 2 Damon Turney 5 Lev Sviridov 5 Balasubramanian Anantharaman 5

1Princeton University Princeton USA2Lawrence Livermore National Laboratory Livermore USA3IBM Yorktown Heights USA4Brookhaven National Laboratory Upton USA5City College of New York New York USA

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9:45 AM - FF4.02
Investigation of Bimetallic Battery Cathode Materials Based on Phosphate and Diphosphate Moieties

Esther S Takeuchi 1 2 3 Amy C Marschilok 2 1 Kenneth J Takeuchi 2

1Stony Brook University Stony Brook USA2Stony Brook University Stony Brook USA3Brookhaven National Laboratory Upton USA

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10:00 AM - FF4.03
Distinct Charge Dynamics in Battery Electrodes Revealed by In Situ and Operando Soft X-Ray Spectroscopy

Xiaosong Liu 1 3 Dongdong Wang 2 Gao Liu 2 Venkat Srinivasan 2 Zhi Liu 1 Zahid Hussain 1 Wanli Yang 1

1Lawrence Berkeley National Laboratory Berkeley USA2Lawrence Berkeley National Laboratory Berkeley USA3Shanghai Institute of Microsystem and Information Technology Shanghai China

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10:15 AM - FF4.04
Understanding Sn-Based Anode Materials for Li-Ion Batteries: X-Ray Absorption Spectroscopic Studies

Qi Wang 1 Zhixin Dong 1 Natasha A. Chernova 1 Fredrick Omenya 1 Hyeyoung Jung 2 Clare P. Grey 2 3 M. Stanley Whittingham 1 2

1State University of New York at Binghamton Binghamton USA2State University of New York at Stony Brook Stony Brook USA3University of Cambridge Cambridge United Kingdom

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10:30 AM - FF4.05
In Operando X-Ray Tomography of Lithium Ion Batteries

Martin Ebner 1 Vanessa Wood 1

1ETH Zurich Zurich Switzerland

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10:45 AM - FF4.06
Observation of Phase Behaviour of LiFePO4 and Li(Fe,Mn)PO4 by Grazing Incidence Diffraction During Cycling of a Lithium Battery

Andrew L Hector 1 Alex Madsen 1 Chris Nicklin 2 John R Owen 1 Michael Palmer 1 Jonathan Rawle 2 Matthew R Roberts 1 3

1University of Southampton Southampton United Kingdom2Diamond Light Source Didcot United Kingdom3Uppsala University Uppsala Sweden

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11:00 AM -
BREAK

11:30 AM - *FF4.07
Operando Methods for Characterization of Fuel Cell and Battery Materials

Hector Abruna 1

1Cornell University Ithaca USA

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12:00 PM - FF4.08
Combining In-Operando X-Ray Diffraction Data with Finite-Element Electrochemical Models of Sodium Metal Halide Cells

Job Rijssenbeek 1 Badri Ramamurthi 1 Svetlana Selezneva 1 Michael Vallance 1 Yan Gao 1 Guillermo Zappi 1 Hui Zhong 2 John B Parise 2 3 4 Zhong Zhong 4

1GE Global Research Niskayuna USA2Stony Brook University Stony Brook USA3Stony Brook University Stony Brook USA4Brookhaven National Laboratory Upton USA

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12:15 PM - FF4.09
In-situ Visualization of Lithium Migration and Internal Structure in Batteries Using X-Ray Compton Scattering

Yoshiharu Sakurai 1 Masayoshi Itou 1 Yuki Orikasa 2 Kousuke Suzuki 3 Hiroshi Sakurai 3 Yoshiharu Uchimoto 2

1Japan Synchrotron Radiation Research Institute Sayo Japan2Kyoto University Kyoto Japan3Gunma University Ota Japan

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