Meetings & Events

spring 1996 logo

1996 MRS Spring Meeting & Exhibit

April 8-12, 1996 | San Francisco
Meeting Chairs
: Thomas F. Kuech, Clifford L. Renschler, Chuang Chuang Tsai



Symposium P: Microporous and Macroporous Materials

Chairs

Jeffrey S. Beck Raul F. Lobo
Mobil Research and Development Corporation University of Delaware

Lennox E. Iton Mark E. Davis
Argonne National Laboratory California Institute of Technology
David R. Corbin Steven L. Suib
E.I. DuPont de Nemours & Co. University of Connecticut

Stacey I. Zones
Chevron Research Company


*Invited Paper

SESSION P1: ZEOLITES, CLAYS AND
MICROPOROUS MATERIALS
Chairs: Mark E. Davis and Stacy Zones
Monday Morning, April 8
Marina C/D

8:15 A.M. P1.1
SYNTHESIS AND CHARACTERIZATION OF OCTAHEDRAL MOLECULAR SIEVES AND LAYERED MATERIALS, Steven L. Suib and Scott R. Segal, University of Connecticut, Departments of Chemistry and Chemical Engineering, Storrs, CT.

8:30 A.M. P1.2
POROUS MATERIALS DERIVED FROM SYNTHETIC POLYMER-CLAY COMPLEXES, K.A. Carrado, Argonne National Laboratory, Chemistry Division, Argonne, IL; P. Thiyagarajan, Argonne National Laboratory, Chemistry and Intense Pulsed Neutron Source Divisions, Argonne, IL; K. Song, D.L. Elder, Argonne National Laboratory, Chemistry Division, Argonne, IL.

8:45 A.M. P1.3
SYNTHESIS OF LAMELLAR ALUMINOPHOSPHATES IN THE PRESENCE OF SURFACTANTS, A. Sayari, I.L. Moudrakovski, J.S. Reddy, V.R. Karra, Université Laval, Chemical Engineering, Sainte-Foy, Canada; and A. Chenite and Y. Le Page, National Research Council of Canada, Ottawa, Canada.

9:00 A.M. *P1.4
AMBIENT ROUTES TO CONTROLLED POROSITY SILICATES: FROM AEROGELS TO MOLECULAR SIEVES, C.J. Brinker, S.S. Prakash, R. Sehgal, N.K. Raman and J. Samuel, The University of New Mexico, Sandia National Laboratories, Albuquerque, NM.

9:30 A.M. P1.5
LOCAL MICROSTRUCTURAL ORGANIZATION IN CARBOGENIC MOLECULAR SIEVES, Henry Foley and Michael Kane, University of Delaware, Department of Chemical Engineering, Newark, NJ.

9:45 A.M. P1.6
STRUCTURAL TEXTURAL AND CATALYTIC PROPERTIES OF Al-Ti AND Al-Zr PILLARED CLAYS, Jose-Manuel Dominguez, Mex-Petrolum Institute, Department of Catalysis and Materials, Mexico, Mexico.

10:00 A.M. *P1.7
THE SYNTHESIS AND CHARACTERIZATION OF METAL SUBSTITUTED UTD-1 MOLECULAR SIEVES, K.J. Balkus Jr, University of Texas at Dallas, Department of Chemistry, Richardson, TX; and S.I. Zones, Chevron Research and Technology, Richmond, CA.

10:30 A.M. BREAK

11:00 A.M. P1.8
THE SYNTHESIS AND CATALYTIC PROPERTIES OF SOME CHIRAL LAYERED AND 3D FRAMEWORK MATERIALS PREPARED USING METAL COMPLEX TEMPLATES, A.P. Wilkinson, D.A. Bruce, M.J. Gray, S.M. Stalder and M.G. White, Georgia Institute of Technology, School of Chemistry and Biochemistry, and School of Chemical Engineering, Atlanta, GA.

11:15 A.M. P1.9
FABRICATION OF RETICULATED CALCIUM PHOSPHATE FRAMEWORKS AND MICROSKELETAL CALCIUM CARBONATE FILMS IN SELF-ORGANISING REACTION MEDIA, Dominic Walsh and Stephen Mann, University of Bath, School of Chemistry, Bath, United Kingdom.

11:30 A.M. *P1.10
SYNTHESIS AND CRYSTAL STRUCTURE OF ULM-16, A NEW OPEN FRAMEWORK FLUORINATED GALLIUM PHOSPHATE WITH 16-RING CHANNELS, Thierry Loiseau and Gérard Férey, Laboratoire des Fluorues and Université du Maine, Department Faculté des Sciences, LeMans, France.

SESSION P2: MESOPOROUS MATERIALS
Chairs: Jeffrey S. Beck and Mark E. Davis
Monday Afternoon, April 8
Marina C/D

1:30 P.M. P2.1
ORGANIC TEMPLATE DESIGN IN THE SYNTHESIS OF MESOPOROUS SILICATE MATERIALS, Qisheng Huo and Galen Stucky, University of California, Santa Barbara, Chemistry Department, Santa Barbara, CA.

1:45 P.M. P2.2
SYNTHESIS AND CHARACTERISATION OF ORDERED MESOPOROUS MATERIALS INCORPORATING ORGAN-SILOXANES, Stephen D. Sims, Sandra L. Burkett and Stephen Mann, University of Batch, School of Chemistry, Bath, United Kingdom.

2:00 P.M. P2.3
DOUBLE LAMELLAR FORMATION IN SILICATE-SURFACTANT MIXTURES, H.-L. Chang and W.-H. Shih, Drexel University, Department of Mechanical Engineering, Philadelphia, PA.

2:15 P.M. P2.4
CATALYTIC HYDROGENATION OF FERMENTATION DERIVED INTERMEDIATES ON MESOPOROUS SILICA SUPPORTED METALS, Y. Wang, J. Lui, J.G. Frye, S. Li and T.A. Werpy, Pacific Northwest National Laboratory, Department of Materials Science, Richland, WA.

2:30 P.M. *P2.5
SYNTHESIS OF MESOPOROUS ALUMINAS, Frederic Vaudry and Mark E. Davis, California Institute of Technology, Department of Chemical Engineering, Pasadena, CA.

3:00 P.M. BREAK

3:30 P.M. *P2.6
IONIC AND NEUTRAL SURFACTANT TEMPLATING OF MESOSTRUCTURED SILICAS AT AMBIENT TEMPERATURE, Wenzhong Zhang and Thomas J. Pinnavaia, Michigan State University, Department of Chemistry, East Lansing, MI.

4:00 P.M. P2.7
NEW DIRECT ROUTE TO MESOPOROUS ALUMINOSILICATES WITH ENHANCED ACIDITY AND CATALYTIC PROPERTIES, R. Mokaya and W. Jones, University of Cambridge, Cambridge, United Kingdom.

4:15 P.M. P2.8
HYDROTHERMAL AND POST-SYNTHESIS INCORPORATION OF TITANIUM INTO MESOPOROUS MCM-48, Mark S. Morey, Galen D. Stucky, Alison Butler, Jerrylaine Walker and Anne Davidson, University of California, Santa Barbara, Department of Chemistry, Santa Barbara, CA.

4:30 P.M. P2.9
MCM-41 TYPE SILICA AS SUPPORT FOR IMMOBILIZED COBALT COMPLEXES, Fethi Bedioui, Emmanuel Briot and Jacques Devynck, Institute of Electrochimie, Paris, France; Kenneth J. Balkus Jr. and Felipe J. Diaz, University of Texas at Dallas, Department of Chemistry, Richardson, TX.

4:45 P.M. P2.10
HEXAGONALLY-PACKED TRANSITION METAL OXIDE MOLECULAR SIEVES, David M. Antonelli and Jackie Y. Ying, Massachusetts Institute of Technology, Department of Chemical Engineering, Cambridge, MA.

POSTER SESSION
Monday Evening, April 8
8:00 P.M.
South Grand Concourse

SESSION P3: ZEOLITES, CLAYS AND
MICROPOROUS MATERIALS

P3.1 DESIGNER CARBONS TEMPLATED BY PILLARED CLAYS: LITHIUM SECONDARY BATTERY ANODES, G. Sandi, R.E. Winans, K.A. Carrado, Argonne National Laboratory, Argonne, IL; P. Thiyagarajan, J.E. Hunt, G.D. Cody, R.E. Botto, Chemistry and IPNS; and G.W. Zajac, Amoco Research Center, Naperville, IL.

P3.2 ENCAPSULATION AND CATALYTIC ACTIVITY OF MANGANESE COMPLEXES IN ZEOLITES, Dirk De Vos, Steven B. Ogunwumi, Julia Meinershagen and Thomas Bein, Purdue University, Department of Chemistry, West Lafayette, IN.

P3.3 ELECTROCHEMICAL CHARATERIZAZTION OF VANADIUM MOLECULAR SIEVE, VAPO-5, Fethi Bedioul, Emmanuel Briot, Jacques Devynck, Institute of Electorchimie, Paris, France; and Kenneth J. Balkus Jr., University of Texas at Dallas, Department of Chemistry, Richardson, TX.

P3.4 SYNTHESIS AND CHARACTERIZATION OF Ln/Al-PILLARD CLAYS, A. Lopez-Ortega, J.M. Dominguez, Instituto Mexicano del Petroleo, Mexico, Mexico; and A. Benitez-Patrico, UNAM, Fac. de Quimica, Mexico, Mexico.

P3.5 SYNTHESIS OF CRYSTALLINE ZINCOSILICATES, Masahito Yoshikawa and Mark E. Davis, California Institute of Technology, Department of Chemical Engineering, Pasadena, CA.

P3.6 ULM-12: THE FIRST SYNTHETIC IRON PHOSPHATE WITH AN OPEN STRUCTURE, Gérard Férey, Myriam Cavellec and Didier Riou, Laboratoire des Fluorues and Université du Maine, Department Faculté des Sciences, LeMans, France.

P3.7 ELECTRICAL BEHAVIOUR OF NATURAL MANGANESE DIOXIDE(MND), Honoria de F Gorgulho, Rosana Z.D. Fernandes and Jean M. Pernaut, UFMG, Quimica, Belo Horizonte, Brazil.

P3.8 POROUS MATERIALS FROM FLY ASH, Jorge Moller and W.-H. Shih, Drexel University, Philadelphia, PA.

P3.9 POROUS MEDIA DEVELOPMENT THROUGH ACID LEACHING OF CERAMIC MATERIAL MADE FROM INDUSTRIAL WASTE, Marcus Fonseca, Pericles Brumati and Regina Nascimento,Instituto de Quimímica, Cidade Universitária, Rio de Janerio, Brazil.

P3.10 IN SITU pH MEASUREMENTS OF HYDROTHERMAL SOLUTIONS, Corine In-Gerardin, In Martin, Lionel Allouche and Francis Taulelle, Louis Pasteur University, NMR and Solid State Chemistry Department, Strasbourg, France.

P3.11 IN SITU NMR INVESTIGATION OF AL(III) HYDROLYSIS AND CONDENSATION UNDER HYDROTHERMAL CONDITIONS, Corine In-Gerardin, Francis Taulelle, Louis Pasteur University, NMR and Solid State Chemistry Debarment, Strasbourg, France; Lionel Allouche, Institut Le Bel, NMR and Solid State Chemistry, Strasbourg, France; and Mohamed Haouas, Louis Pasteur University, NMR and Solid State Chemistry, Strasbourg, France.

P3.12 ELECTROCHEMICAL Li INSERTION IN LAYERED AND TUNNEL-STRUCTURE MANGANESE OXIDES, L.F. Nazar, M.J. Duncan and F. Leroux, University of Waterloo, Department of Chemistry, Waterloo, Canada.

SESSION P4: MESOPOROUS MATERIALS

P4.1 SYNTHESIS OF PERIODIC MESOPOROUS GELS, Mark T. Anderson, James E. Martin, Judy Odinek and Paula Newcomer, Sandia National Laboratories, Albuquerque, NM.

P4.2 MICELLIZATION AND PERIODICITY IN SURFACTANT-TEMPLATED MESOPOROUS SILICA, James E. Martin, Mark T. Anderson, Judy Odinek and Paula Newcomer, Sandia National Laboratories, Albuquerque, NM.

P4.3 MESOSTRUCTURED ZIRCONIUM OXIDE, J.S. Reddy, P. Liu and A. Sayari, Université Laval, Department of Chemical Engineering, Sainte-Foy, Canada.

P4.4 BIOMIMETIC TEMPLATING OF POROUS LAMELLAR SILICAS BY VESICULAR SURFACTANT ASSEMBLIES, Peter T. Tanev and Thomas J. Pinnavaia, Michigan State University, Department of Chemistry and Center for Fundamental Materials Research, East Lansing, MI.

P4.5 INFLUENCE OF SYNTHESIS PARAMETERS ON TEXTURAL AND STRUCTURAL PROPERTIES OF MCM-41 MESOPOROUS MATERIALS, E. Terres, S.S. Ramirez, J.M. Dominguez, A. Muntoya and J. Navarrete, Instituto Mexicano del Petróleo, Goia de Catálisis y Materials, Mexico, Mexico.

P4.6 EFFECT OF SILICON/ALUMINUM MOLAR RATIOS ON THE FORMATION OF ALUMINOSILICATE MESOPOROUS MOLECULAR SIEVES, H.-L. Chang and W.-H. Shih, Drexel University, Department of Mechanical Engineering, Philadelphia, PA.

P4.7 EMISSION CONTROL CATAYLSTS DERIVED FROM MESOPOROUS MOLECULAR SIEVES, Partha P. Paul, Michael A. Miller, Martin J. Heimrich and Stuart T. Schwab, Southwest Research Institute, San Antonio, TX.

P4.8 COOPERATIVE CONTROL OF PHASE TRANSITIONS IN SILICATE MESOSTRUCTURES, Christopher C. Landry, Galen D. Stucky, University of California, Santa Barbara; Department of Chemistry, Santa Barbara, CA; Alain Monnier, Universite de Geneve, Chimie Physique Sciences II, Geneva, Switzerland; Jon C. Hanson and Paul Norby, Brookhaven National Laboratory, Department of Chemistry, Upton, NY.

P4.9 CHARACTERIZATION OF BAMBOO AS A NATURAL GRADIENT POROUS MATERIAL, I.G. Solorzano, Department of Materials Science and Engineering, Rio De Janeiro, Brazil; and K. Ghavami, PUC-Rio, Department of Civil Engineering, Rio De Janeiro, Brazil.

P4.10 NANOCRYSTALLINE MESOPOROUS TiO2 ELECTRODES FOR PHOTOVOLTAIC APPLICATIONS, Christophe Barbé and Michael Graetzel, Swiss Federal Institute of Technology, Institute of Physical Chemistry, Lausanne, Switzerland.

SESSION P5: METHODS OF STUDYING POROSITY
Chairs: Lennox Iton and Raul Lobo
Tuesday Morning, April 9
Marina C/D

8:30 A.M. P5.1
THE BAND AT 960, Stephan Schwarz, David R. Corbin and Alexander J. Vega, DuPont Central Research and Development, Wilmington, DE.

8:45 A.M. P5.2
MONTE CARLO SIMULATIONS OF XENON IN ZEOLITES AND THE 129Xe NMR CHEMICAL SHIFT, V. Gupta, H.T. Davis and A.V. McCormick, University of Minnesota, Department of Chemical Engineering and Material Science, Minneapolis, MN.

9:00 A.M. P5.3
COMPETITIVE ADSORPTION OF MOLECULAR ADSORBATES ON Cu-ZSM-5: A COMBINED IN SITU FTIR SPECTROSCOPIC AND THEORETICAL STUDY, Janos Szanyi, Mark Paffett, Los Alamos National Laboratory, CST Division, Los Alamos, NM; Holman Brand and Antonio Redondo, Los Alamos National Laboratory, Theoretical Division, Los Alamos, NM.

9:15 A.M. P5.4
POTENTIALITIES OF INNOVATIVE TECHNIQUES LIKE Xe NMR AND SAXS FOR THE CHARACTERIZATION OF MICROPOROUS SOL-GEL DERIVED SiO2, Anne Julbe, CNRS-UM II-ENSCM, Lab. des Materiaux et Procedes Membranaires, Montpellier, France; Herve Jobic, CNRS, Institut de Recherches sur la Catalyse, Villeurbanne, France; Louis-Charles De Menorval, CNRS-ENSCM, Lab. des Materiaux Catalytiques et Catalyse en Chimie Organique, Montpellier, France; and Christian Guizard, CNRS-UM II-ENSCM, Lab. des Materiaux et Procedes Membranaires, Montpellier, France.

9:30 A.M. P5.5
SPECTROSCOPY OF METAL GERMANIUM SULFIDE FRAMEWORK MATERIALS AND PRECURSORS, Scott J. Kirkby and Geoffrey A. Ozen, University of Toronto, Materials Chemistry Research Group, Lash Miller Chemical Laboratories, Ontario, Canada.

9:45 A.M. P5.6
POROUS SILICON STRUCTURAL EVOLUTION FROM IN-SITU LUMINESCENCE AND RAMAN MEASUREMENTS, David R. Tallant, Michael J. Kelly, Terry R. Guilinger and Regina L. Simpson, Sandia National Laboratories, Albuquerque, NM.

10:00 A.M. *P5.7
PROBING THE BINDING SITES OF ADSORBED MOLECULES IN ACIDIC AND BASIC ZEOLITES WITH SOLID STTE NMR SPECTROSCOPY, Clare Grey, Hsien-Ming Kao, State University of New York at Stony Brook, Department of Chemistry, Stony Brook, NY.

10:30 A.M. BREAK

11:00 A.M. P5.8
PREPARATION OF MICROPOROUS FILMS WITH SUB NANOMETER PORES AND THEIR CHARACTERIZATION USING STRESS AND FTIR MEASUREMENTS, J. Samuel, A.J. Hurd, C.J. Brinker and S.C. Contakes, Sandia National Laboratories Albuquerque, Ceramic Processing Science Department, Albuquerque, NM.

11:15 A.M. P5.9
MORPHOLOGICAL CHARACTERIZATION OF MICROPOROUS CARBON MATERIALS, M. Singh, NYMA, Inc., Lewis Research Center Group, Cleveland, OH; and S.C. Farmer, NASA Lewis Research Center, Cleveland, OH.

11:30 A.M. P5.10
A NEW ADSORPTION TECHNIQUE FOR PROBING PORE SIZE AND DIMENSIONALITY OF MOLECULAR SIEVES, J.S. Geilfuss, L.T., Yuen and S.I. Zones, Chevron Research and Technology Company, Richmond, CA.

11:45 A.M. P5.11
STRUCTURES AND DYNAMICS OF FUNCTIONAL MOLECULES IN POROUS CERAMICS STUDIED USING MULTINUCLEAR SOLID STATE NUCLEAR MAGNETIC RESONANCE, Li-Qiong Wang, J. Liu, W.D. Samuels and G.J. Exarhos, Pacific Northwest National Laboratory, Materials Science Department, Richland, WA.

SESSION P6: THIN FILMS AND ADSORPTION
Chairs: Steven L. Suib and Stacey Zones
Tuesday Afternoon, April 9
Marina C/D

1:30 P.M. P6.1
PREPARATION OF CaTiO3 FILMS ON POROUS Al2O3 SUBSTRATES, Eugene A. Pruss, Mark J. Hampden-Smith, University of New Mexico, Department of Chemistry, Albuquerque, NM; and Timothy Ward, University of New Mexico, University of New Mexico, Albuquerque, NM.

1:45 P.M. P6.2
DEVELOPMENT OF CHEMICALLY FUNCTIONALIZED CARBON SUBSTRATES FOR CRYSTALLIZATION OF MOLECULAR SIEVE FILMS, Kathleen Hoekstra and Thomas Bein, Purdue University, Department of Chemistry, West Lafayette, IN.

2:00 P.M. P6.3
GROWTH AND ENGINEERING OF MICROPOROUS ZEOLITE FILMS AND COATINGS, Y. Yan, S. Ray Chaudhuri and A. Sarkar, YTC American Inc., Camarillo, CA.

2:15 P.M. P6.4
IN SITU SYNTHESIS OF PERIODIC MESOPOROUS THIN FILMS, Mark T. Anderson, James E. Martin, Judy Odinek and Paula Newcomer, Sandia National Laboratories, Albuquerque, NM.

2:30 P.M. *P6.5
PREPARATION OF MEMBRANES FROM ZEOLITE NANOSOLS AND USE OF SECONDARY GROWTH, Michael Tsapatsis, Mark C. Lovallo and Laura C. Boudreau, University of Massachusettes, Department of Chemical Engineering, Goessmann Laboratory, Amherst, MA.

3:00 P.M. BREAK

3:30 P.M. P6.6
ZEOLITE: MEMBRANES FROM KAOLIN, B.G. Karle, University of New Mexico, Advanced Materials Laboratory, Albuquerque, NM; C.J. Brinker and M.L.F. Phillips, Sandia National Laboratories, Advanced Materials Laboratory, Albuquerque, NM.

3:45 P.M. P6.7
SYNTHESIS OF MEOSOPOROUS AND ZEOLITIC FILMS THROUGH LIQUID-LIQUID INTERFACIAL REACTIONS, J.R. Bontha, A.Y. Kim and J. Liu, Battelle Pacific Northwest National Laboratories, Department of Materials Science, Richland, WA.

4:00 P.M. P6.8
GAS PERMEABILITY AND SORPTION IN SOL-GEL DERIVED MICRO-AND MESOPOROUS SILICA MATERIALS, L.W. Hrubesh, P.R. Coronado and J.F. Poco, Lawrence Livermore National Laboratory, Chemistry and Materials Science Department, Livermore, CA.

4:15 P.M. P6.9
SPECIAL HYSTERESIS EFFECTS in N2-SORPTION AND Hg-POROSIMETRY MEASUREMENTS, Herbert Giesche, New York State College of Ceramics at Alfred University, Alfred, NY.

4:30 P.M. P6.10
MICROSTRUCTURAL ANALYSIS OF THIN POROUS SILICON LAYERS WITH VARIABLE ANGLE SPECTROSCOPIC ELLIPSOMETRY, Leif Pettersson, Hans Arwin, Shahin Zangooie and Robert Bjorklund, Linköping University, Department of Physics and Measurement Technology, Linköping, Sweden.

4:45 P.M. P6.11
NONOSTRUCTURAL STUDY OF LUMINESCENT POROUS POLYCRYSTALLINE SILICON THIN FILMS, Vincent M.C. Poon, P.G. Han, University of Science, Electrical Engineering, Hong Kong.

POSTER SESSION
Tuesday Evening, April 9
8:00 P.M.
Presidio Ballroom

SESSION P7: METHODS OF STUDYING POROSITY

P7.1 X-RAY LUMINESCENCE OF DISPERSE SiO2 AND POROUS SILICON, V.Ya. Degoda, S.N. Naumenko, Kiev University, Physical Department, Kiev, Ukraine; Yu.D. Glinka and V.M. Ogenko, Institute of Surface Chemistry, Kiev, Ukraine.

P7.2 CHARACTERISATION OF PORES IN Al2O3 FILMS FOR HIGH SENSITIVITY HUMIDITY SENSOR, R.K. Nahar and P.D. Vyas, Central Electronics Engineering Research Institute, Pilani, India.

P7.3 ADSORPTION ENERGY DISTRIBUTION EVALUATION OF MESOPOROUS ADSORBENTS FROM LASER SPECTROSCOPY MEASUREMENTS, Yu.D. Glinka, Institute of Surface Chemistry of the National Academy of Science of Ukraine, Kiev, Ukraine.
P7.4 NMR STUDIES OF CEMENTS, CONCRETE AND RELATED MATERIALS, Orest Jarh, Ana Sepe, Peter Jevinkar, Nenad Funduk, "Jozef Stefen Institute", Ljubljana, Slovenia; Renato Toffanin and Vladimir Mlynarik, Area Research Centre, Trieste, Italy.

P7.5 DO ALKALI METAL ANIONS (M) EXIST IN ZEOLITE A? Peter D. Barker, Peter P. Edwards and Paul A. Anderson, University of Birmingham, School of Chemistry, Birmingham, United Kingdom.

P7.6 MATHEMATICAL MODELING OF ZEOLITE GROWTH: THE ROLE OF PRECURSOR GEL MICROSTRUCTURE, Michael Tsapatsis and Dionisios G. Vlachos, University of Massachusetts, Goessmann Laboratory, Amherst, MA.

P7.7 WATER POROSIMETRY - A NEW TECHNIQUE FOR CHARACTERIZATION OF HYDROPHOBIC POROUS SOLIDS, Alexander, Fadeev, Pavel Ustynyuk, George Lisichkin, Moscow State University, Chemistry Department, Moscow, Russia; and Valentine Eroshenko, Polytechnical Institute, Kiev, Ukraine.

P7.8 IN SITU NMR DURING HYDROTHERMAL SYNTHESES OF ULMS INSTRUMENTATION, pH MEASUREMENTS AND CONDENSATION MECHANISMS, Francis B.L. Taulelle, Corine In-Gerardin and Martin In, Louis Pasteur University, NMR and Solid State Chemistry, Strasbourg, France.

P7.9 NEUTRON VIBRATIONAL SPECTROSCOPIC STUDIES OF THE H5O2+ ION AND ITS D-EXCHANGED ANALOGS IN DODECATUNGSTOPHOSPHORIC ACID HEXAHYDRATE, N.C. Maliszewskyj, T.J. Udovic, J.M. Nicol, National Institutes of Standards and Technology, Gaithersburg, MD.

P7.10 APPLICATIONS OF NEUTRON SCATTERING FOR THE STUDY OF MICRO- AND MACROPOROUS MATERIALS, N.C. Maliszewskyj, National Institutes of Standards and Technology, Gaithersburg, MD.

SESSION P8: THIN FILMS AND ADSORPTION

P8.1 A NEW CLASS OF MICROPOROUS MATERIALS: POROUS METAL PHOSPHONATE THIN FILMS, L.A. Vermeulen, S. Burgmeyer, T. Fisher, M. Hansford and J. Pattanayak, Southern Illinois University, Department of Chemistry and Biochemistry, Carbondale, IL.

P8.2 THIN LAYER ALUMINUM POROUS FILMS AND COATINGS ON SUBSTRATES, Victor Kedrov, Gennadiy Strukov and Geliy Nechiporenko, Institute of Chemical Physics in Chernogolovka, Russian Academy of Sciences, Moscow, Russia.

SESSION P9: SOL-GEL SYNTHESIS OF
METAL OXIDES AND NITRIDES
Chairs: Jeffrey S. Beck and David R. Corbin
Wednesday Morning, April 10
Marina C/D

8:30 A.M. P9.1
MICROPOROUS METAL-ORGANIC SOLIDS, Omar Yaghi and Hialian Li, Arizona State University, Department of Chemistry and Biochemistry, Tempe, AZ.

8:45 A.M. P9.2
SOL-GEL POLYMERIZATION OF TETRAALKOXYGERMANIUM AND ORGANOTRIALKOXYGERMANIUM COMPOUNDS, Brigitta M. Baugher and Douglas A. Loy, Sandia National Laboratories, Properties of Organic Materials Department, Albuquerque, NM.

9:00 A.M. P9.3
SYNTHESIS AND STRUCTURAL STUDY OF MICROPOROUS YTTRIA-STABILIZED ZIRCONIA CERAMICS, Ram Srinivasan and Burtron Davis, University of Kentucky, Lexington, KY.

9:15 A.M. P9.4
CHARACTERIZATION OF PORE MORPHOLOGY IN POROUS SILICON, M. Cruz, I.P.N., ESIME-UC, Mexico, Mexico; M.R. Beltrán, C. Wang, University of Mexico, Instituto de Investigaciones en Materials, Mexico, Mexico and J. Tagüeña-Martínez, University of Mexico, Laboratory Energía Solar-IIM, Mexico, Mexico.

9:30 A.M. P9.5
PROTEINS ENCAPSULATED IN POROUS SOL-GELS: BIOMOLECULES AS PORE STRUCTURE TEMPLATES, Bakul C.Dave, Bruce Dunn, University of California, Department of Materials Science and Engineering, Los Angeles, CA; Joan S. Valentine and Jeffrey I. Zink, University of California, Department of Chemistry and Biochemistry, Los Angeles, CA.

9:45 A.M. P9.6
NON-POLAR PROCESSING OF SILICA SOL-GEL MATERIALS VIA A COMBINED INVERSE MICELLE/SOL-GEL TECHNIQUE, Stacey A. Yamanaka, Anthony Martino, Jeffrey S. Kawola and Douglas A. Loy, Sandia National Laboratories, Albuquerque, NM.

10:00 A.M. *P9.7
CHEMICAL SYNTHESIS AND NITRIDATION OF NANOMETER SIZED CERAMIC POWDERS, L.K. Kurihara, G.M. Chow, P.E. Schoen, Naval Research Laboratory, Center for Bio/Molecular Science and Engineering, Washington, DC.

10:30 A.M. BREAK

11:00 A.M. P9.8
AEROGEL SYNTHESIS USING EXTRACTIVE DRYING, D.M. Smith, W.C. Ackerman, T. Romero, NanoPore Incorporated, Albuquerque, NM; A. Zimmerman and F. Schwertfegar, Hoechst, Frankfurt, Germany.

11:15 A.M. P9.9
A RAPID SUPERCRITICAL EXTRACTION PROCESS FOR THE PRODUCTION OF SILICA AEROGELS, J.F. Poco, P.R. Coronado, R.W. Pekala and L.W. Hrubesh, Lawrence Livermore National Laboratory, Chemistry and Materials Science Department, Livermore, CA.

11:30 A.M. P9.10
POROUS-SILICA DOPING BY ION BOMBARDMENT, Gianfranco Cerofolini, Laura Meda, EniChem, Istituto Guido Donegani, Novara, Italy.

11:45 A.M. P9.11
MICROPOROUS AEROGELS AS HOST MATRICES FOR GALLIUM NITRIDE NANOCLUSTERS, Timothy J. Goodwin, Mark Niemeyer, Valerie J. Leppert, Christine A. Smith, Philip P. Power, Subhash H. Risbud, University of California, Davis, Davis, CA; Howard W.H. Lee and Lawrence W. Hrubesh, Lawrence Livermore National Laboratory, Livermore, CA.

SESSION P10: APPLICATIONS OF POROUS METAL OXIDES
Chairs: Lennox Iton and Raul Lobo
Wednesday Afternoon, April 10
Marina C/D

1:30 P.M. *P10.1
OPTICAL STUDIES OF LOW DENSITY SILICA AEROGELS, Sally A. Cahill, University of California, Davis, Department of Applied Sciences, Davis CA; Howard W.H. Lee and Lawrence R. Hrubesh, Lawrence Livermore National Laboratory, Livermore, CA.

2:00 P.M. P10.2
SOL-GEL PROCESS FROM HETEROMETALLIC ALKOXIDE TO INCORPORATE ALKALINE-AND RARE EARTHS IN ALUMINA FOR AUTOMOTIVE APPLICATIONS, C.K. Narula, Ford Motor Company, Department of Chemistry, Dearborn, MI.

2:15 P.M. P10.3
SYTHESIS CHARACTERIZATION AND CATALYTIC PROPERTIES OF Al2O3-TiO2 MIXED OXIDES PREPARED BY SOL-GEL, Jose-Manuel Dumincuez and J. Melendez, Mex-Petrolum Institute, Department of Catalysis and Materials, Mexico, Mexico.

2:30 P.M. P10.4
GAS PERMEATION AND MICROSTRUCTURE OF SILICA MEMBRANES PREPARED BY SOL-GEL PROCESSING, G.Z. Cao, N.K. Raman, R. Sehgal and C.J. Brinker, Advanced Materials Laboratory, Albuquerque, NM.

2:45 P.M. P10.5
SOL-GEL PROCESSED ALUMINA BASED MATERIALS IN MICROCALORIMETER SENSOR DEVICE FABRICATION FOR AUTOMOTIVE APPLICATIONS, S.R. Nakouzi, Ford Motor Company, Chemistry Department, Dearborn, MI; J. McBride, Ford Motor Company, Physics Department, Dearborn, MI; and C.K. Narula, Ford Motor Company, Chemistry Department, Dearborn, MI.

3:00 P.M. BREAK

3:30 P.M. P10.6
NANOCHANNEL GLASS REPLICA MEMBRANES FOR PARALLEL PATTERNING APPLICATIONS, D.H. Pearson, R.J. Tonucci and C.R. Eddy Jr., Naval Research Laboratory, Washington, DC.

3:45 P.M. P10.7
OPTICAL AND ELECTRONIC PROPERTIES OF SILICON NANOCLUSTERS WITH PASSIVATED SURFACES, L.N. Dinh, University of California, Davis-Livermore, Department of Applied Science and Lawrence Livermore National Laboratory, Chemistry and Materials Science, Livermore, CA; L.L. Chase, M. Balooch, W. Siekhaus, Lawrence Livermore National Laboratory, Chemistry and Materials Science, Livermore, CA; and F. Wooten Olivera, University of California Davis-Livermore, Department of Applied Science, Livermore, CA.

4:00 P.M. P10.8
HIGH-PASS OPTICAL FILTERS BASED ON GOLD-COATED NANOCHANNEL GLASS MATERIALS, A. Rosenberg and R.J. Tonucci, Naval Research Laboratory, Washington, DC.

4:15 P.M. P10.9
OPTICAL INTERFERENCE FILTERS MADE OF POROUS SILICON, M. Thönissen, M.G. Berger, M. Krüger, R. Arens-Fischer, O. Glück, S. Billat, H. Lüth, Institut für Schicht- und Ionentechnik, Forschungszentrum, Jülich, Germany; W. Theiß, S. Hilbrich and P. Grosse, RWTH Aachen, Aachen, Germany.

4:30 P.M. P10.10
INFLUENCE OF THERMAL EXPANSION MISMATCH ON RESIDUAL STRESSES AND FLOW RESPONSE OF MICROBALLOON COMPOSITES, Ming. Y. He, M. Kiser, B. Wu and F.W. Zok, University of California, Santa Barbara, Materials Department, Santa Barbara, CA.

4:45 P.M. P10.11
OPTICAL AND STRUCTURAL PROPERTIES OF POROUS SILICON, Paulo Ventura, University of Aveiro, Department of Physics, Aveiro, Portugal; Kevin O'Donnell, Strath Clyde University, Department of Physics, Glasgow, United Kingdom; and Jose Gracio, University of Aveiro, Department of Medical Engineering, Aveiro, Portugal.

POSTER SESSION
Wednesday Evening, April 10
8:00 P.M.
Presidio Ballroom

SESSION P11: SOL-GEL SYNTHESIS OF
METAL OXIDES AND NITRIDES

P11.1 INFLUENCE OF ELECTROLYTE NATURE ON MICROSTRUCTURE OF POROUS ALUMINUM ANODIC OXIDE FILMS, Victor Surganov and Gennadij Gorokh,Belorussian State University of Informatics and Radioelectronics, Minsk, Belarus.

P11.2 INVESTIGATION OF SOL-GEL ROUTE IN THE SYNTHESIS OF LITHIUM ION CONDUCTING GLASSES, N. Satyanarayana, Pondicherry University, Raman School of Physics, Pondicherry, India; M. Venkateswarlu, Osmania University, Department of Physics, Hyderabad, India; and P. Muralidharan, Pondicherry University, Raman School of Physics, Pondicherry, India.

P11.3 Si3N4 WHISKER UPPER LAYER FORMATION ON SiC-Al2O3 POROUS BODY, P. Toro, A. Pérez, G. Baeza, Universidad de Chile, Basic Chemistry Department, Santiago, Chile; G. Piderit and P. Rojas, Comisión Chilena Energía Nuclear, Santiago, Chile.

P11.4 CHARACTERIZATION OF POROUS A1N SEPARATORS FOR BATTERIES, H. Giesche, B.N. Thorsland, NYSCC at Alfred University, Alfred, NY; T.J. Mroz and M. Martin, Advanced Refractory Technologies, Buffalo, NY.

P11.5 MESOPOROUS ZIRCONIA BY COOPERATIVE INTERCALATION OF THE ZIRCONIA PRECURSOR AND AMPHOTERIC SURFACTANT, A.Y. Kim, P.J. Bruinsma, Y.L. Chen and J.Liu, Pacific Northwest National Laboratory, Department of Materials Science, Richland, WA.

P11.6 CHEMICAL MODIFICATION OF SILICA AEROGELS BY TREATMENT WITH MICROWAVE ENERGIZED GASES, Michael R. Ayers and Arlon J. Hunt, Lawrence Berkeley National Laboratory, Energy and Environment Division, Berkeley, CA.

SESSION P12: APPLICATIONS OF POROUS METAL OXIDES


P12.1 EFFECT OF PREPARATION PARAMETERS IN THE MICROPOROUS STRUCTURE OF Ni/SiO2 CATALYSTS, F.F. Castillon, N. Bodganchikova, Instituto de Física UNAM Laboratorio, Ensenada Baja California, México; and S. Fuentes, Instituto de Física UNAM Laboratorio, Ensenada, México and Centro de Investigaciones y de Estudios Superiores de Ensenada (CISESE) Ensenada Baja California, México.

P12.2 ORDERED NANOMAGNETS BASED ON MESOPOROUS SILICA, Y. Wang, M. Qian, Y.L. Chen, A.Y. Kim and J. Liu, Pacific Northwest National Laboratory, Department of Materials Science, Richland, WA.

P12.3 COMBINED TEXTURE STUDY OF BASE CATALYZED SILICA AEROGELS BY TEM, SAXS AND POROSIMETRY: FRACTAL APPROACH, Yuri I. Aristov, Natalia V. Lisitza, Aleksey G. Okunev, Boreskov Institute of Catalysis, Novosibirsk, Russia; Jaroslav Lorenz and Andrzej B. Jarzebski, Institute of Chemical Engineering, Gliwice, Poland.

SESSION P13: POROUS SEMICONDUCTORS

P13.1 DEPOSITION OF GaAs AND InAs INTO UNIFORM NANOCHANNEL GLASS CAPILLARY ARRAYS, R.J. Tonucci and A.D. Berry, Naval Research Laboratory, Washington, DC.

P13.2 CHARACTERIZATION OF THE POROUS BORON -DOPED Si SUPERLATTICE, Ting-Chang Chang, National Nano Device Laboratory, Hsin-Chu Taiwan; Yu-Jan Mei, Wen-Chung Tsai, Jeng-Dong Sheu, Wen-Kuan Yeh, Chun-Yen Chang, National Chiao Tung University, Department of Electronics Engineering and Institute of Electronics, Hsin-Chu, Taiwan.

P13.3 MICROSTRUCTURAL AND CHEMICAL EFFECTS ON THE ELECTROCHEMICAL BEHAVIOR OF CARBON AEROGEL CAPACITORS, John M. Miller, Bruce Dunn, University of California, Los Angeles, Department of Materials Science and Engineering, Los Angeles, CA; and R.W. Pekala, Lawrence Livermore National Laboratory, Chemistry and Materials Science Department, Livermore, CA.

P13.4 THE MORPHOLOGY STRUCTURE AND PHYSICAL PROPERTIES OF POROUS GaAs LAYERS, Yu.N. Buzynin, S.A. Gusev, M.N. Drozdov, Yu.N. Drozdov, Z.F. Krastilnik, A.V. Murel, D.G. Revin, V.I.Shashkin and I.Yu. Shuleshova, Russian Academy of Science, Institute for Physics of Microstructures, Nizhny Novgorod, Russia.

P13.5 ACTIVATED CARBON FILAMENTS OF DIAMETER ~0.1 um, Weiming Lu, D.D.L. Chung, State University of New York at Buffalo, Composite Materials Research Laboratory, Buffalo, NY; and Christine A. Frysz, Wilson Greatbatch Limited, Clarence NY.

P13.6 CARBON AEROGEL ELECTRODES FOR CAPACITIVE DEIONIZATION, R.W. Pekala, J.K. Nielsen, D.V. Fix, G.V. Mack and J.C. Farmer, Lawrence Livermore National Laboratory, Chemistry and Materials Science Department, Livermore, CA.

P13.7 GRAPHIIZED NEEDLE COKES AND NATURAL GRAPHITES FOR LITHIUM INTERCALATION, T.D. Tran, W. Pekala Lawrence Livermore National Laboratory, Chemistry and Materials Science Department, Livermore, CA; W.M. Goldberger, Superior Graphite Company, Chicago, IL; W.M. Goldberger, Superior Graphite Company, Chicago, IL; X. Song, Lawrence Berkeley National Laboratory, Energy and Environment Division, Berkeley, CA; and K. Kinoshita, Lawrence Berkeley National Laboratory, Energy and Environment Division, Berkeley, CA.

P13.8 EFFECT OF PROCESSING VARIABLES ON THE MICROSTRUCTURE AND FLEXURAL PROPERTIES OF MICROPOROUS CARBON MATERIALS, M. Singh and R.F. Dacek, NYMA, Inc., Lewis Research Center Group, Cleveland, OH.

SESSION P14: POROUS POLYMERS

P14.1 MORPHOLOGICAL CHARACTERIZATION OF FURFURALDEHYDE RESINS ADSORBENTS, Ruben R. Sanchez, Sergio Neves Monteiro, State University North of Rio de Janeiro (UENF), Rio de Janeiro, Brazil; and Jose R. D'Almeida, Rio de Janeiro Catholic University, Rio de Janeiro, Brazil.

P14.2 IMPROVING THERMAL PERFORMANCE OF HIGH INTERNAL PHASE EMULSION POLYMERIZED FOAMS WITH MALEIMIDE BASED MONOMERS, Mark Hoisington, Joseph Duke and David Langlois, Los Alamos National Laboratory, Materials Science and Technology Division, Polymers and Coatings Group, Los Alamos, NM.

SESSION P15: POROUS SEMICONDUCTORS
Chair: David R. Corbin
Thursday Morning, April 11
Marina C/D

8:30 A.M. P15.1
PREPARATION AND CHARACTERIZATION OF THIN POROUS ELECTRODES BY AEROSOL SPRAY PYROLYSIS (ASP), W. Wang and E.E. Hellstrom, University of Wisconsin-Madison, Madison, WI.

8:45 A.M. P15.2
TAILORING POROSITY IN POLYMER-DERIVED SiC, Jon F. Nebo, University of New Mexico, Center for Micro-Engineered Ceramics, Albuquerque, NM; Cathy S. Scotto, Sandia National Laboratories, Advanced Materials Laboratory, Albuquerque, NM; A. Bennett, University of Toledo, Department of Chemical Engineering, Toledo, OH; and C. Jeffrey Brinker, University of New Mexico, Center for Micro-Engineered Ceramics, Albuquerque, NM and Sandia National Laboratories, Advanced Materials Laboratory, Albuquerque, NM.

9:00 A.M. P15.3
BICONTINUOUS CUBIC PHASE AS A MESOPOROUS MATRIX FOR THE SYNTHESIS OF NANOCRYSTALLINE II-VI SEMICONDUCTORS, Jianping Yang, Georgetown University, Washington, DC; Syed Qadri and Banahalli Ratna, Naval Research Laboratory, Center for Bio/Molecular Science and Engineering, Washington, DC.

9:15 A.M. P15.4
FABRICATION AND CHARACTERIZATION OF METALLIC AND MAGNETIC NANOWIRE ARRAYS WITH NOVEL PROPERTIES, P.P. Nguyen and R.J. Tonucci, Naval Research Lab, Washington, DC.

9:30 A.M. P15.5
POROSITY AND GRAIN SIZE CONTROL TO OPTIMIZE THE GAS SENSING PROPERTIES ZINC OXIDE USING RATE CONTROLLED SINTERING, Gaurav Agarwal and Robert F. Speyer, Georgia Institute of Technology, School of Materials Science and Engineering, Atlanta, GA.

9:45 A.M. P15.6
FROM GRAPHITE TO POROUS CARBON CONTAINING NANOPARTICLES THROUGH CHEMICAL REACTIONS, Ching-cheh Hung, NASA Lewis Research Center, Electro-Physics Branch, Cleveland, OH; and Jean Corbin, Cleveland State University, Department of Chemistry, Cleveland, OH.

10:00 A.M. *P15.7
FORMATION AND PROPERTIES OF POROUS GaAs, Patrik Schmuki, Michael Graham, National Research Council, Institution for Microstructural Science, Ottawa, Canada; and Hugh Isaacs, Brookhaven National Laboratory, Department of Applied Sciences, Upton, NY.

10:30 A.M. BREAK

11:00 A.M. P15.8
PHOTONIC BAND STRUCTURE OF NANOCHANNEL GLASS MATERIALS, A. Rosenberg, R.J. Tonucci, H.-B. Lin, Naval Research Laboratory, Washington, DC; and Eric L. Shirley, National Institute of Standards and Technology, Gaithersburg, MD.

11:15 A.M. P15.9
COLLOIDAL PROCESSING OF TEMPERATURE SHOCK RESISTANT SiC WITH TAILORED POROSITY, Mesut Aslan, Rüdiger Nass, Helmut Schmidt, INM Im Stadtwald, Ceramic department, Saarbücken, Germany.

11:30 A.M. P15.10
A COMPARISON OF THE ELECTROCHEMICAL BEHAVIOR OF CARBON AEROGELS AND ACTIVATED CARBON FIBER CLOTHS, T.D. Tran, C.T. Alviso, J.K. Nielsen and R.W. Pekala, Lawrence Livermore National Laboratory, Chemistry and Materials Science Department, Livermore, CA.

11:45 A.M. P15.11
ELECTRONIC DOPING IN POROUS NANO-CRYSTALLINE ZnO FILMS, R. Könenkamp and A. Wahi, Hahn-Meitner Institut, Berlin, Germany.

SESSION P16: POROUS POLYMERS
Chair: Steven L. Suib
Thursday Afternoon, April 11
Marina C/D

1:30 P.M. P16.1
NANOFOAM POROSITY MEASURED BY INFRARED SPECTROSCOPY AND REFRACTIVE INDEX, Martha Sanchez, J.L. Hedrick and T.P. Russell, IBM Almaden Research Center, San Jose, CA.

1:45 P.M. P16.2
TAILORING THE PORE SIZE OF HYPERCROSSLINKED POLYMER FOAMS, W.P. Steckel Jr., M.A. Mitchell and P.G. Apen, Los Alamos National Laboratory, Los Alamos, NM.

2:00 P.M. P16.3
NANOPOROUS POLYIMIDE FILMS FROM POLYIMIDE-ALIPHATIC POLYESTER OR POLYIMIDE-ALIPHATIC POLYCARBONATE COPOLYMERS, K.R. Carter, J.L. Hedrick, R. Richter, IBM Almaden Research Center, San Jose, CA; D. Mecerreyes and R. Jérôme, Université de l'Etat a Liége, Liége, Belgium.

2:30 P.M. P16.4
MECHANICAL PROPERTY AND PERMEABILITY STUDIES ON RESORCINOL-FORMALDEHYDE GELS, G. Scherer, E. I. duPont de Nemours & Co., Inc., Central Research and Development, Wilmington, DE; C.T. Alviso and R.W. Pekala, Lawrence Livermore National Laboratory, Chemistry and Materials Science Department, Livermore, CA.

2:45 P.M. P16.5
HETEROGENEOUS MICROCOMPOSITE MATERIALS BASED ON POROUS MATRICES AND LIQUID CRYSTALS, F.M. Aliev, V.V. Nadtotchi and G.P. Sinha, University of Puerto Rico, Department of Physics and Materials Research Center, San Juan, PR.

3:00 P.M. BREAK

3:30 P.M. P16.6
MICROPOOUS SILOXANE ELASTOMERS FOR PACKAGING INTERCONNECTIONS, TESTING AND BURN-IN APPLICATIONS, D.M. Alberta, C.J.G. Plummer, J.G. Hilborn, Swiss Federal Institute of Technology, Lausanne, Materials Department, Polymer Laboratory, Lausanne, Switzerland; J.L. Hedrick, R.D. Miller and D.Y. Shih, IBM Almaden Research Center, San Jose, CA.

3:45 P.M. P16.7
SYNTHESIS AND CHARACTERIZATION OF WELL-DEFINED POROUS CROSS-LINKED DI- AND TRIBLOCK COPOLYMERS PREPARED VIA RING OPENING METATHESIS POLYMERIZATION, Randall S. Saunders, James H. Small and Robert R. Lagasse, Sandia National Laboratories, Albuquerque, NM.

4:00 P.M. P16.8
RESORCINOL-FORMALDEHYDE AEROGEL MICROSPHERES, Cynthia T. Alviso, Richard W. Pekala, Lawrence Livermore National Laboratory, Chemistry and Materials Science Department, Livermore, CA; Xianping Lu, Roland Caps and Jochen Fricke, Physikalisches Institut, Universität, Würzburg, Germany.

4:15 P.M. P16.9
MACROPOROUS THERMOSETS VIA CHEMICALLY INDUCED PHASE SEPARATION, J. Kiefer, J.G. Hilbom, Swiss Federal Institute of Technology, Materials Department, Polymers Laboratory, Lausanne, Switzerland; and J.L. Hedrick, IBM Almaden Research Center, San Jose, CA.

4:30 P.M. P16.10
ELECTROSYNTHESIS AND CHARACTERIZATION OF POROUS POLYCYCLOPHOSPHAZENE LAYERS, Jing Li and Mira Josowicz, Pacific Northwest National Laboratory, Materials Research Center, Richland, WA.


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See page 6 for a complete list of exhibitors.